3-(aminomethyl)-6-methyl-4-(phenylmethyl)-2(1H)-pyridinone hydrochloride

Base Information

Chemical Name:3-(aminomethyl)-6-methyl-4-(phenylmethyl)-2(1H)-pyridinone hydrochloride
CAS No.:1346576-17-7
Molecular Formula:C₁₄H₁₆N₂O*ClH
Molecular Weight:264.755
Hs Code.:

Synonyms:3-(aminomethyl)-6-methyl-4-(phenylmethyl)-2(1H)-pyridinone hydrochloride

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Chemical Property of 3-(aminomethyl)-6-methyl-4-(phenylmethyl)-2(1H)-pyridinone hydrochloride

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Technology Process of 3-(aminomethyl)-6-methyl-4-(phenylmethyl)-2(1H)-pyridinone hydrochloride

There total 4 articles about 3-(aminomethyl)-6-methyl-4-(phenylmethyl)-2(1H)-pyridinone hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1346576-24-6
1,1-dimethylethyl {[6-methyl-2-oxo-4-(phenylmethyl)-1,2-dihydro-3-pyridinyl]methyl}carbamate

: 1346576-17-7
3-(aminomethyl)-6-methyl-4-(phenylmethyl)-2(1H)-pyridinone hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 60 ℃; for 1h;

Reference yield: 86.0%

: 1346576-21-3
3-(aminomethyl)-6-methyl-4-(phenylmethyl)-2(1H)-pyridinone

: 1346576-17-7
3-(aminomethyl)-6-methyl-4-(phenylmethyl)-2(1H)-pyridinone hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 60 ℃; for 1h;

Reference yield:

: 101-97-3
Ethyl 2-phenylethanoate

: 1346576-17-7
3-(aminomethyl)-6-methyl-4-(phenylmethyl)-2(1H)-pyridinone hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium amide / diethyl ether / -5 - 20 °C / Reflux; Inert atmosphere

1.2: pH 4 - 5

2.1: piperidine / ethanol / 75 °C / Reflux

2.2: 12 h / 2327.23 Torr / Inert atmosphere; Sealed vessel

2.3: 4 h / 0 - 20 °C

3.1: hydrogenchloride / 1,4-dioxane / 1 h / 60 °C

With piperidine; hydrogenchloride; sodium amide; In 1,4-dioxane; diethyl ether; ethanol;