(E)-1-(methyl(phenyl)(vinyl)silyl)-2-(1',3',2'-dioxaborinan-2'-yl)ethene

Base Information

Chemical Name:(E)-1-(methyl(phenyl)(vinyl)silyl)-2-(1',3',2'-dioxaborinan-2'-yl)ethene
CAS No.:1228307-56-9
Molecular Formula:C₁₄H₁₉BO₂Si
Molecular Weight:258.2
Hs Code.:

Synonyms:(E)-1-(methyl(phenyl)(vinyl)silyl)-2-(1',3',2'-dioxaborinan-2'-yl)ethene

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Chemical Property of (E)-1-(methyl(phenyl)(vinyl)silyl)-2-(1',3',2'-dioxaborinan-2'-yl)ethene

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Technology Process of (E)-1-(methyl(phenyl)(vinyl)silyl)-2-(1',3',2'-dioxaborinan-2'-yl)ethene

There total 4 articles about (E)-1-(methyl(phenyl)(vinyl)silyl)-2-(1',3',2'-dioxaborinan-2'-yl)ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 17983-32-3
methyl(phenyl)(divinyl)silane

: 5,5--dimethyl--2--vinyl-1,3,2-dioxaborinane

: 1228307-56-9
(E)-1-(methyl(phenyl)(vinyl)silyl)-2-(1',3',2'-dioxaborinan-2'-yl)ethene

: 1228307-57-0
bis[(E)-2-(1',3',2'-dioxaborinan-2'-yl)ethen-1-yl](methyl)(phenyl)silane

Guidance literature:: With carbonylchlorohydridobis(tricyclohexylphosphine)ruthenium(II); In toluene; at 80 ℃; for 24h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.jorganchem.2010.02.019

Reference yield: 37.0%

: 17983-32-3
methyl(phenyl)(divinyl)silane

: 5,5--dimethyl--2--vinyl-1,3,2-dioxaborinane

: 1228307-56-9
(E)-1-(methyl(phenyl)(vinyl)silyl)-2-(1',3',2'-dioxaborinan-2'-yl)ethene

: 1228307-54-7
1-(methyl(phenyl)(vinyl)silyl)-1-(1',3',2'-dioxaborinan-2'-yl)ethene

: 1228307-57-0
bis[(E)-2-(1',3',2'-dioxaborinan-2'-yl)ethen-1-yl](methyl)(phenyl)silane

Guidance literature:: With carbonylchlorohydridobis(tricyclohexylphosphine)ruthenium(II); In toluene; at 25 ℃; for 24h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.jorganchem.2010.02.019

Reference yield: 24.0%

: 17983-32-3
methyl(phenyl)(divinyl)silane

: 5,5--dimethyl--2--vinyl-1,3,2-dioxaborinane

: 1228307-56-9
(E)-1-(methyl(phenyl)(vinyl)silyl)-2-(1',3',2'-dioxaborinan-2'-yl)ethene

Guidance literature:: carbonylchlorohydridobis(tricyclohexylphosphine)ruthenium(II); In toluene; Ru complex, toluene, borinane (1.7 mmol) and silane (1.7 mmol) derivs. placed in glass ampoule under Ar at 80°C for 48 h; isolated using silica gel column (hexane/ethyl acetate = 4/1); elem. anal.;
DOI:10.1016/j.jorganchem.2010.02.019