(4S,5R)-4-benzyloxy-5-hydroxy-N-(4-methoxybenzyl)-7-methyloctanoyl amide

Base Information

Chemical Name:(4S,5R)-4-benzyloxy-5-hydroxy-N-(4-methoxybenzyl)-7-methyloctanoyl amide
CAS No.:1160427-41-7
Molecular Formula:C₂₄H₃₃NO₄
Molecular Weight:399.53
Hs Code.:

Synonyms:(4S,5R)-4-benzyloxy-5-hydroxy-N-(4-methoxybenzyl)-7-methyloctanoyl amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,5R)-4-benzyloxy-5-hydroxy-N-(4-methoxybenzyl)-7-methyloctanoyl amide

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Technology Process of (4S,5R)-4-benzyloxy-5-hydroxy-N-(4-methoxybenzyl)-7-methyloctanoyl amide

There total 2 articles about (4S,5R)-4-benzyloxy-5-hydroxy-N-(4-methoxybenzyl)-7-methyloctanoyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1160427-05-3
C₂₄H₃₁NO₄

: 1160427-41-7
(4S,5R)-4-benzyloxy-5-hydroxy-N-(4-methoxybenzyl)-7-methyloctanoyl amide

Guidance literature:: With zinc(II) tetrahydroborate; In diethyl ether; at -20 - 20 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2009.03.021

Reference yield:

: 763105-88-0
(S)-3-benzyloxy-1-(4-methoxybenzyl)-2,6-piperidinedione

: 1160427-41-7
(4S,5R)-4-benzyloxy-5-hydroxy-N-(4-methoxybenzyl)-7-methyloctanoyl amide

: 1220911-49-8
(4S,5S)-4-benzyloxy-5-hydroxy-N-(4-methoxybenzyl)-7-methyloctanoylamide

Guidance literature:: (S)-3-benzyloxy-1-(4-methoxybenzyl)-2,6-piperidinedione; i-butylmagnesium halide;

With L-Selectride; In tetrahydrofuran; at -20 - 20 ℃; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.3390/molecules15042771