N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl]phosphonous diamide

Base Information

• Chemical Name: N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl]phosphonous diamide
• CAS No.: 1232774-39-8
• Molecular Formula: C₁₀H₁₁Cl₃F₃N₂P
• Molecular Weight: 353.539

Synonyms:N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl]phosphonous diamide

Chemical Property of N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl]phosphonous diamide

Chemical Property:

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Technology Process of N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl]phosphonous diamide

There total 1 articles about N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl]phosphonous diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-trifluoromethylphenylamine (455-14-1) + N,N-dimethyl-P-(trichloromethyl)phosphonamidous chloride (79650-12-7) → N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl]phosphonous diamide (1232774-39-8)

Guidance literature:

With pyridine; triethylamine; In benzene; at 0 - 18 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2010.03.087

Reference yield: 85.0%

N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl]phosphonous diamide (1232774-39-8) → N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl] phosphonoselenoic diamide (1232774-57-0)

Guidance literature:

With pyridine; selenium; at 20 ℃; for 15h; Inert atmosphere;

DOI:10.1016/j.tet.2010.03.087

Reference yield: 78.0%

N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl]phosphonous diamide (1232774-39-8) → N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl]phosphonothioic diamide (1232774-49-0)

Guidance literature:

With pyridine; sulfur; at 16 ℃; for 72h; Inert atmosphere;

DOI:10.1016/j.tet.2010.03.087

upstream raw materials:

4-trifluoromethylphenylamine

N,N-dimethyl-P-(trichloromethyl)phosphonamidous chloride

Downstream raw materials:

N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl]-phosphonic diamide

N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl]phosphonothioic diamide

N,N-dimethyl-P-(trichloromethyl)-N'-[4-(trifluoromethyl)-phenyl] phosphonoselenoic diamide

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