1-nitro-5,6,7,8-tetrahydro-2-naphthalenamine

Base Information

• Chemical Name: 1-nitro-5,6,7,8-tetrahydro-2-naphthalenamine
• CAS No.: 342043-42-9
• Molecular Formula: C₁₀H₁₂N₂O₂
• Molecular Weight: 192.217
• Mol file: 342043-42-9.mol

Synonyms:2-amino-1-nitro-5,6,7,8-tetrahydronaphthalene

Chemical Property of 1-nitro-5,6,7,8-tetrahydro-2-naphthalenamine

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

1-NITRO-5,6,7,8-TETRAHYDRONAPHTHALEN-2-AMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-nitro-5,6,7,8-tetrahydro-2-naphthalenamine

There total 11 articles about 1-nitro-5,6,7,8-tetrahydro-2-naphthalenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

N-(1-nitro-5,6,7,8-tetrahydro-2-naphthalenyl)acetamide (104509-00-4) → 2-amino-1-nitro-5,6,7,8-tetrahydronaphthalene (342043-42-9)

Guidance literature:

With sulfuric acid; water; In ethanol; at 20 ℃; for 1h; Reflux;

DOI:10.1002/cmdc.201100284

Reference yield:

tetralin (119-64-2) → 2-amino-1-nitro-5,6,7,8-tetrahydronaphthalene (342043-42-9)

Guidance literature:

Multi-step reaction with 5 steps

1: sulfuric acid; nitric acid / 0 °C

2: hydrogen; nickel; tetralin

3: water

4: sulfuric acid; glacial acetic acid; nitric acid / <45

5: alcoholic hydrochloric acid

With hydrogenchloride; tetralin; sulfuric acid; water; hydrogen; nitric acid; nickel; acetic acid;

Reference yield:

6-nitrotetralin (19353-86-7) → 2-amino-1-nitro-5,6,7,8-tetrahydronaphthalene (342043-42-9)

Guidance literature:

Multi-step reaction with 4 steps

1: hydrogen; nickel; tetralin

2: water

3: sulfuric acid; glacial acetic acid; nitric acid / <45

4: alcoholic hydrochloric acid

With hydrogenchloride; tetralin; sulfuric acid; water; hydrogen; nitric acid; nickel; acetic acid;

upstream raw materials:

N-(1-nitro-5,6,7,8-tetrahydro-2-naphthalenyl)acetamide

ethanol

5,6-dinitro-1,2,3,4-tetrahydro-naphthalene

N-(5,6,7,8-tetrahydronaphth-2-yl)acetamide

Downstream raw materials:

N₂-methyl-5,6,7,8-tetrahydronaphthalene-1,2-diamine

N-methyl-1-nitro-5,6,7,8-tetrahydronaphthalen-2-amine

C₂₀H₁₇N₃

N-(1-nitro-5,6,7,8-tetrahydro-[2]naphthyl)-toluene-4-sulfonamide