(E)-4-(5'-hydroxy-2',6',6'-trimethyl-1'-cyclohexen-1'-yl)-3-buten-2-one ethylene acetal

Base Information

Chemical Name:(E)-4-(5'-hydroxy-2',6',6'-trimethyl-1'-cyclohexen-1'-yl)-3-buten-2-one ethylene acetal
CAS No.:85198-01-2
Molecular Formula:C₁₅H₂₄O₃
Molecular Weight:252.354
Hs Code.:

Synonyms:(E)-4-(5'-hydroxy-2',6',6'-trimethyl-1'-cyclohexen-1'-yl)-3-buten-2-one ethylene acetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-(5'-hydroxy-2',6',6'-trimethyl-1'-cyclohexen-1'-yl)-3-buten-2-one ethylene acetal

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Technology Process of (E)-4-(5'-hydroxy-2',6',6'-trimethyl-1'-cyclohexen-1'-yl)-3-buten-2-one ethylene acetal

There total 2 articles about (E)-4-(5'-hydroxy-2',6',6'-trimethyl-1'-cyclohexen-1'-yl)-3-buten-2-one ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 85198-00-1
(E)-3-(3',3'-ethylendioxy-1'-butenyl)-2,2,4-trimethyl-3-cyclohexen-1-one

: 85198-01-2
(E)-4-(5'-hydroxy-2',6',6'-trimethyl-1'-cyclohexen-1'-yl)-3-buten-2-one ethylene acetal

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 ℃; for 1h;
DOI:10.1002/hlca.19820650802

Reference yield:

: 85197-97-3
(E)-5-(3',3'-ethylendioxy-1'-butenyl)-4,6,6-trimethyl-2,4-cyclohexadien-1-one

: 85198-01-2
(E)-4-(5'-hydroxy-2',6',6'-trimethyl-1'-cyclohexen-1'-yl)-3-buten-2-one ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / lithium trimethoxyaluminum hydride, CuBr / tetrahydrofuran / 1.5 h / -20 - -15 °C

2: 98 percent / NaBH₄ / ethanol / 1 h / 0 °C

With sodium tetrahydroborate; lithium trimethoxyaluminohydride; copper(I) bromide; In tetrahydrofuran; ethanol;
DOI:10.1002/hlca.19820650802