3-Buten-2-one, 4-(5-hydroxy-2,6,6-trimethyl-1-cyclohexen-1-yl)-, (E)-

Base Information

Chemical Name:3-Buten-2-one, 4-(5-hydroxy-2,6,6-trimethyl-1-cyclohexen-1-yl)-, (E)-
CAS No.:66465-74-5
Molecular Formula:C13H20O2
Molecular Weight:208.29700
Hs Code.:

Synonyms:3-Buten-2-one,4-(5-hydroxy-2,6,6-trimethyl-1-cyclohexen-1-yl)-,(E);4-(5'-hydroxy-2',2',6'-trimethylcyclohex-1'-enyl)but-3-en-2-on;

Suppliers and Price of 3-Buten-2-one, 4-(5-hydroxy-2,6,6-trimethyl-1-cyclohexen-1-yl)-, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-Buten-2-one, 4-(5-hydroxy-2,6,6-trimethyl-1-cyclohexen-1-yl)-, (E)-

Chemical Property:

PSA：37.30000
LogP:2.62900

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Buten-2-one, 4-(5-hydroxy-2,6,6-trimethyl-1-cyclohexen-1-yl)-, (E)-

There total 13 articles about 3-Buten-2-one, 4-(5-hydroxy-2,6,6-trimethyl-1-cyclohexen-1-yl)-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 85198-01-2
(E)-4-(5'-hydroxy-2',6',6'-trimethyl-1'-cyclohexen-1'-yl)-3-buten-2-one ethylene acetal

: 66465-74-5
4-(5'-hydroxy-2',2',6'-trimethylcyclohex-1'-enyl)but-3-en-2-on

Guidance literature:: With Dowex 50 (H⁽¹⁺⁾); In acetone; for 1h;
DOI:10.1002/hlca.19820650802

Reference yield:

: 4-<5'-(1''-ethoxyethoxy)-2',2',6'-trimethylcyclohex-1'-enyl>but-3-en-2-on

: 66465-74-5
4-(5'-hydroxy-2',2',6'-trimethylcyclohex-1'-enyl)but-3-en-2-on

Guidance literature:: With hydrogenchloride; In acetone; for 0.5h; Ambient temperature;
DOI:10.1002/hlca.19890720312

Reference yield:

: 85198-00-1
(E)-3-(3',3'-ethylendioxy-1'-butenyl)-2,2,4-trimethyl-3-cyclohexen-1-one

: 66465-74-5
4-(5'-hydroxy-2',2',6'-trimethylcyclohex-1'-enyl)but-3-en-2-on

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaBH₄ / ethanol / 1 h / 0 °C

2: 93 percent / Dowex 50 (H⁽¹⁺⁾) / acetone / 1 h

With sodium tetrahydroborate; Dowex 50 (H⁽¹⁺⁾); In ethanol; acetone;
DOI:10.1002/hlca.19820650802