octyl 2,3,4-tri-O-benzyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

Base Information

Chemical Name:octyl 2,3,4-tri-O-benzyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside
CAS No.:397249-86-4
Molecular Formula:C₆₂H₇₄O₁₁
Molecular Weight:995.263
Hs Code.:

Synonyms:octyl 2,3,4-tri-O-benzyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

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Chemical Property of octyl 2,3,4-tri-O-benzyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

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Technology Process of octyl 2,3,4-tri-O-benzyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

There total 3 articles about octyl 2,3,4-tri-O-benzyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 397249-85-3
octyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

: 397249-86-4
octyl 2,3,4-tri-O-benzyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1.5h;
DOI:10.1248/cpb.49.1464

Reference yield:

: octyl 2,3,4-tri-O-benzyl-β-D-galactopyranoside

: 397249-86-4
octyl 2,3,4-tri-O-benzyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / MS-AW₃₀₀; NIS; TfOH / various solvent(s) / 0.17 h / -60 °C

2: 86 percent / Bu₄NF / tetrahydrofuran / 1.5 h / 20 °C

With N-iodo-succinimide; trifluorormethanesulfonic acid; MS-AW₃₀₀; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1248/cpb.49.1464

Reference yield:

: 397249-84-2
phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-thio-β-D-galactopyranoside

: 397249-86-4
octyl 2,3,4-tri-O-benzyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / MS-AW₃₀₀; NIS; TfOH / various solvent(s) / 0.17 h / -60 °C

2: 86 percent / Bu₄NF / tetrahydrofuran / 1.5 h / 20 °C

With N-iodo-succinimide; trifluorormethanesulfonic acid; MS-AW₃₀₀; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1248/cpb.49.1464