phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-thio-β-D-galactopyranoside

Base Information

• Chemical Name: phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-thio-β-D-galactopyranoside
• CAS No.: 397249-84-2
• Molecular Formula: C₃₉H₄₈O₅SSi
• Molecular Weight: 656.959

Synonyms:phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-thio-β-D-galactopyranoside

Chemical Property of phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-thio-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-thio-β-D-galactopyranoside

There total 1 articles about phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

benzyl bromide (100-39-0) + phenyl 6-O-(tert-butyldimethylsilyloxy)-1-thio-β-D-galactopyranoside (225241-29-2) → phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-thio-β-D-galactopyranoside (397249-84-2)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 2h;

DOI:10.1248/cpb.54.485

Reference yield: 91.0%

octyl 2,3,4-tri-O-benzyl-β-D-galactopyranoside + phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-thio-β-D-galactopyranoside (397249-84-2) → octyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside (397249-85-3)

Guidance literature:

With N-iodo-succinimide; trifluorormethanesulfonic acid; MS-AW₃₀₀; In various solvent(s); at -60 ℃; for 0.166667h;

DOI:10.1248/cpb.49.1464

Reference yield: 81.2%

N-(2,2,2-trichloroethoxycarbonyl)hexanolamine (146292-94-6) + phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-thio-β-D-galactopyranoside (397249-84-2) → 6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-galactopyranoside (898528-01-3)

Guidance literature:

With N-iodo-succinimide; trifluorormethanesulfonic acid; MSAW-300; In various solvent(s); at -60 ℃; for 1h;

DOI:10.1248/cpb.54.485

upstream raw materials:

benzyl bromide

phenyl 6-O-(tert-butyldimethylsilyloxy)-1-thio-β-D-galactopyranoside

Downstream raw materials:

octyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-galactopyranoside

6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-α/β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-β-D-galactopyranoside

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 397249-84-2 phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-thio-β-D-galactopyranoside

Send

Send

Metric Ton KG G Pound L ML

Send

Send