acetyl tris(pentafluorophenyl)germane

Base Information

• Chemical Name: acetyl tris(pentafluorophenyl)germane
• CAS No.: 191978-52-6
• Molecular Formula: C₂₀H₃F₁₅GeO
• Molecular Weight: 616.809
• Mol file: 191978-52-6.mol

Synonyms:acetyl tris(pentafluorophenyl)germane

Chemical Property of acetyl tris(pentafluorophenyl)germane

Chemical Property:

Purity/Quality:

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Technology Process of acetyl tris(pentafluorophenyl)germane

There total 1 articles about acetyl tris(pentafluorophenyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

tris-(pentafluor phenyl) germyl lithium (191978-54-8) + Acetyl bromide (506-96-7) → acetyl tris(pentafluorophenyl)germane (191978-52-6)

Guidance literature:

In tetrahydrofuran; -60°C;

DOI:10.1016/S0022-328X(96)06677-6

Reference yield:

1-iodo-butane (542-69-8) + acetyl tris(pentafluorophenyl)germane (191978-52-6) → n-hexan-2-one (591-78-6) + dimethylglyoxal (431-03-8)

Guidance literature:

In benzene-d6; for 3h; Title compound not separated from byproducts; Ambient temperature; Irradiation;

DOI:10.1016/S0022-328X(96)06677-6

upstream raw materials:

tris-(pentafluor phenyl) germyl lithium

Acetyl bromide

Downstream raw materials:

n-hexan-2-one

dimethylglyoxal