tert-butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-(tert-butyldiphenylsilanyloxy)valerate

Base Information

Chemical Name:tert-butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-(tert-butyldiphenylsilanyloxy)valerate
CAS No.:1404378-85-3
Molecular Formula:C₃₆H₄₅NO₆Si
Molecular Weight:615.842
Hs Code.:

Synonyms:tert-butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-(tert-butyldiphenylsilanyloxy)valerate

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Chemical Property of tert-butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-(tert-butyldiphenylsilanyloxy)valerate

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Technology Process of tert-butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-(tert-butyldiphenylsilanyloxy)valerate

There total 4 articles about tert-butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-(tert-butyldiphenylsilanyloxy)valerate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1404378-84-2
tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-hydroxyvalerate

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1404378-85-3
tert-butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-(tert-butyldiphenylsilanyloxy)valerate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

Reference yield:

: 90719-32-7
(S)-4-Benzyl-2-oxazolidinone

: 1404378-85-3
tert-butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-(tert-butyldiphenylsilanyloxy)valerate

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / chloroform / 20 °C / Cooling with ice

2.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 - -50 °C

2.2: -78 - -15 °C

3.1: hydrogen / palladium(II) hydroxide / ethyl acetate; tetrahydrofuran / 4.5 h / 760.05 Torr

4.1: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 °C

With 1H-imidazole; dmap; hydrogen; sodium hexamethyldisilazane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium(II) hydroxide; In tetrahydrofuran; chloroform; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 169897-87-4
[4S]-4-benzyl-3-(4-benzyloxy-1-butanoyl)-2-oxazolidinone

: 1404378-85-3
tert-butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-(tert-butyldiphenylsilanyloxy)valerate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 - -50 °C

1.2: -78 - -15 °C

2.1: hydrogen / palladium(II) hydroxide / ethyl acetate; tetrahydrofuran / 4.5 h / 760.05 Torr

3.1: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 °C

With 1H-imidazole; hydrogen; sodium hexamethyldisilazane; palladium(II) hydroxide; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide;