tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-hydroxyvalerate

Base Information

Chemical Name:tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-hydroxyvalerate
CAS No.:1404378-84-2
Molecular Formula:C₂₀H₂₇NO₆
Molecular Weight:377.437
Hs Code.:

Synonyms:tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-hydroxyvalerate

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Chemical Property of tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-hydroxyvalerate

Chemical Property:

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Technology Process of tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-hydroxyvalerate

There total 3 articles about tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-hydroxyvalerate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1404378-83-1
tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-benzyloxyvalerate

: 1404378-84-2
tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-hydroxyvalerate

Guidance literature:: With hydrogen; palladium(II) hydroxide; In tetrahydrofuran; ethyl acetate; for 4.5h; under 760.051 Torr;

Reference yield:

: 90719-32-7
(S)-4-Benzyl-2-oxazolidinone

: 1404378-84-2
tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-hydroxyvalerate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / chloroform / 20 °C / Cooling with ice

2.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 - -50 °C

2.2: -78 - -15 °C

3.1: hydrogen / palladium(II) hydroxide / ethyl acetate; tetrahydrofuran / 4.5 h / 760.05 Torr

With dmap; hydrogen; sodium hexamethyldisilazane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium(II) hydroxide; In tetrahydrofuran; chloroform; ethyl acetate;

Reference yield:

: 169897-87-4
[4S]-4-benzyl-3-(4-benzyloxy-1-butanoyl)-2-oxazolidinone

: 1404378-84-2
tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-hydroxyvalerate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 - -50 °C

1.2: -78 - -15 °C

2.1: hydrogen / palladium(II) hydroxide / ethyl acetate; tetrahydrofuran / 4.5 h / 760.05 Torr

With hydrogen; sodium hexamethyldisilazane; palladium(II) hydroxide; In tetrahydrofuran; ethyl acetate;