3-O-allyl-1,2,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranose

Base Information

• Chemical Name: 3-O-allyl-1,2,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranose
• CAS No.: 869648-84-0
• Molecular Formula: C₄₉H₄₂O₉
• Molecular Weight: 774.867
• Mol file: 869648-84-0.mol

Synonyms:3-O-allyl-1,2,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranose

Chemical Property of 3-O-allyl-1,2,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranose

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-O-allyl-1,2,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranose

There total 3 articles about 3-O-allyl-1,2,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3R,4S,5R,6R)-4-Allyloxy-6-trityloxymethyl-tetrahydro-pyran-2,3,5-triol + benzoyl chloride (98-88-4) → 3-O-allyl-1,2,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranose (869648-84-0)

Guidance literature:

With pyridine; at 20 ℃; for 24h;

DOI:10.1016/j.carres.2005.08.010

Reference yield:

trityl chloride (76-83-5) → 3-O-allyl-1,2,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranose (869648-84-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 48 h / 20 °C

2: 29.8 g / pyridine / 24 h / 20 °C

With pyridine;

DOI:10.1016/j.carres.2005.08.010

Reference yield:

3-O-allyl-D-glucopyranose (91109-44-3) → 3-O-allyl-1,2,4-tri-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranose (869648-84-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 48 h / 20 °C

2: 29.8 g / pyridine / 24 h / 20 °C

With pyridine;

DOI:10.1016/j.carres.2005.08.010

upstream raw materials:

benzoyl chloride

trityl chloride

3-O-allyl-D-glucopyranose

Downstream raw materials:

C₃₇H₅₀O₉

lauryl 6-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranoside

6-O-acetyl-3-O-allyl-2,4-di-O-benzoyl-α-D-glucopyranosyl trichloroacetimidate

C₃₂H₃₀O₁₀