(S)-tert-butyl-4-((16-(benzyloxy)hexadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

Base Information

Chemical Name:(S)-tert-butyl-4-((16-(benzyloxy)hexadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate
CAS No.:1353667-09-0
Molecular Formula:C₃₄H₅₉NO₅
Molecular Weight:561.846
Hs Code.:

Synonyms:(S)-tert-butyl-4-((16-(benzyloxy)hexadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

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Chemical Property of (S)-tert-butyl-4-((16-(benzyloxy)hexadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

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Technology Process of (S)-tert-butyl-4-((16-(benzyloxy)hexadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

There total 4 articles about (S)-tert-butyl-4-((16-(benzyloxy)hexadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 108149-63-9,108149-65-1
tert-butyl (4S)-4-(hydroxymethyl)-2,2-dimethyl-1,3-oxazolidine-3-carboxylate

: 188180-39-4
2-(16-benzyloxyhexadec-1-yl)bromide

: 1353667-09-0
(S)-tert-butyl-4-((16-(benzyloxy)hexadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2011.10.117

Reference yield:

: C₂₃H₄₀O₂

: 1353667-09-0
(S)-tert-butyl-4-((16-(benzyloxy)hexadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0.75 h / 0 - 20 °C

2: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 12 h / 0 - 20 °C

With carbon tetrabromide; tetra-(n-butyl)ammonium iodide; sodium hydride; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2011.10.117

Reference yield:

: 7735-42-4
1,16-hexadecanediol

: 1353667-09-0
(S)-tert-butyl-4-((16-(benzyloxy)hexadecyloxy)methyl)-2,2-dimethyloxazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 12 h / 0 - 20 °C

2: carbon tetrabromide; triphenylphosphine / dichloromethane / 0.75 h / 0 - 20 °C

3: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 12 h / 0 - 20 °C

With carbon tetrabromide; tetra-(n-butyl)ammonium iodide; sodium hydride; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.10.117