Technology Process of 2-(4-Allyloxybenzyl)phenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside
There total 6 articles about 2-(4-Allyloxybenzyl)phenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
dichloromethane;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: magnesium / iodine / tetrahydrofuran
2.1: tetrahydrofuran / 0.5 h / 20 °C
3.1: sodium hydroxide; Dess-Martin periodane / dichloromethane; water / 1 h / 0 - 20 °C
4.1: hydrogenchloride / ethanol / 20 °C
5.1: triethylamine; methyl chloroformate / tetrahydrofuran / 1.5 h / 0 - 20 °C
5.2: 2.5 h / 0 - 20 °C
6.1: boron trifluoride diethyl etherate / dichloromethane / 2 h / 20 °C
With
hydrogenchloride; sodium hydroxide; boron trifluoride diethyl etherate; Dess-Martin periodane; magnesium; triethylamine; methyl chloroformate;
iodine;
In
tetrahydrofuran; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide; Dess-Martin periodane / dichloromethane; water / 1 h / 0 - 20 °C
2.1: hydrogenchloride / ethanol / 20 °C
3.1: triethylamine; methyl chloroformate / tetrahydrofuran / 1.5 h / 0 - 20 °C
3.2: 2.5 h / 0 - 20 °C
4.1: boron trifluoride diethyl etherate / dichloromethane / 2 h / 20 °C
With
hydrogenchloride; sodium hydroxide; boron trifluoride diethyl etherate; Dess-Martin periodane; triethylamine; methyl chloroformate;
In
tetrahydrofuran; ethanol; dichloromethane; water;
