{1-[(2S,4S)-2-((S)-2,3-Dimethoxy-propyl)-[1,3]dioxolan-4-ylmethyl]-2-methyl-propenyloxy}-dimethyl-phenyl-silane

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Chemical Name:{1-[(2S,4S)-2-((S)-2,3-Dimethoxy-propyl)-[1,3]dioxolan-4-ylmethyl]-2-methyl-propenyloxy}-dimethyl-phenyl-silane
CAS No.:129156-00-9
Molecular Formula:C₂₁H₃₄O₅Si
Molecular Weight:394.583
Hs Code.:

Synonyms:{1-[(2S,4S)-2-((S)-2,3-Dimethoxy-propyl)-[1,3]dioxolan-4-ylmethyl]-2-methyl-propenyloxy}-dimethyl-phenyl-silane

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Chemical Property of {1-[(2S,4S)-2-((S)-2,3-Dimethoxy-propyl)-[1,3]dioxolan-4-ylmethyl]-2-methyl-propenyloxy}-dimethyl-phenyl-silane

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Technology Process of {1-[(2S,4S)-2-((S)-2,3-Dimethoxy-propyl)-[1,3]dioxolan-4-ylmethyl]-2-methyl-propenyloxy}-dimethyl-phenyl-silane

There total 16 articles about {1-[(2S,4S)-2-((S)-2,3-Dimethoxy-propyl)-[1,3]dioxolan-4-ylmethyl]-2-methyl-propenyloxy}-dimethyl-phenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 766-77-8
Dimethylphenylsilane

: 129155-98-2
1-[(2S,4S)-2-((S)-2,3-Dimethoxy-propyl)-[1,3]dioxolan-4-yl]-3-methyl-but-3-en-2-one

: 129156-00-9
{1-[(2S,4S)-2-((S)-2,3-Dimethoxy-propyl)-[1,3]dioxolan-4-ylmethyl]-2-methyl-propenyloxy}-dimethyl-phenyl-silane

Guidance literature:: Wilkinson's catalyst; at 55 ℃;
DOI:10.1016/S0040-4020(01)81981-5

Reference yield: 90.0%

: 766-77-8
Dimethylphenylsilane

: 129155-97-1
1-[(2R,4S)-2-((S)-2,3-Dimethoxy-propyl)-[1,3]dioxolan-4-yl]-3-methyl-but-3-en-2-one

: 82780-44-7,129155-99-3,129156-00-9
{1-[(2R,4S)-2-((S)-2,3-Dimethoxy-propyl)-[1,3]dioxolan-4-ylmethyl]-2-methyl-propenyloxy}-dimethyl-phenyl-silane

Guidance literature:: Wilkinson's catalyst; at 55 ℃; for 1h;
DOI:10.1016/S0040-4020(01)81981-5

Reference yield:

: 129155-91-5
(S)-3,4-dimethoxybutan-1-ol

: 82780-44-7,129155-99-3,129156-00-9
{1-[(2R,4S)-2-((S)-2,3-Dimethoxy-propyl)-[1,3]dioxolan-4-ylmethyl]-2-methyl-propenyloxy}-dimethyl-phenyl-silane

Guidance literature:: Multi-step reaction with 7 steps

1: 98 percent / oxalyl chloride, DMSO, N-methylmorpholine / CH₂Cl₂ / 2.5 h / 0 °C

2: 66 percent / TsOH, MgSO₄ / CH₂Cl₂ / 48 h / Ambient temperature

3: 88 percent / liq. ammonia, sodium / diethyl ether / 0.5 h / -78 °C

4: 50 percent / pyridinium chlorochromate, celite / CH₂Cl₂ / 2.5 h / 20 °C

5: 88 percent / tetrahydrofuran / 0.17 h

6: pyridinium chlorochromate, celite / CH₂Cl₂ / 3.5 h

7: 90 percent / 3P>3RhCl / 1 h / 55 °C

With 4-methyl-morpholine; oxalyl dichloride; Celite; ammonia; sodium; magnesium sulfate; toluene-4-sulfonic acid; dimethyl sulfoxide; pyridinium chlorochromate; Wilkinson's catalyst; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)81981-5