(R)-3-Benzyloxymethoxy-tetradecanoic acid (R)-1-[(2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-benzyloxymethoxy-hexadecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxycarbonylmethyl]-dodecyl ester

Base Information

Chemical Name:(R)-3-Benzyloxymethoxy-tetradecanoic acid (R)-1-[(2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-benzyloxymethoxy-hexadecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxycarbonylmethyl]-dodecyl ester
CAS No.:126024-97-3
Molecular Formula:C₇₃H₁₁₇NO₁₃
Molecular Weight:1216.73
Hs Code.:

(R)-3-Benzyloxymethoxy-tetradecanoic acid (R)-1-[(2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-benzyloxymethoxy-hexadecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxycarbonylmethyl]-dodecyl ester

Synonyms:(R)-3-Benzyloxymethoxy-tetradecanoic acid (R)-1-[(2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-benzyloxymethoxy-hexadecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxycarbonylmethyl]-dodecyl ester

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Chemical Property of (R)-3-Benzyloxymethoxy-tetradecanoic acid (R)-1-[(2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-benzyloxymethoxy-hexadecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxycarbonylmethyl]-dodecyl ester

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Technology Process of (R)-3-Benzyloxymethoxy-tetradecanoic acid (R)-1-[(2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-benzyloxymethoxy-hexadecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxycarbonylmethyl]-dodecyl ester

There total 3 articles about (R)-3-Benzyloxymethoxy-tetradecanoic acid (R)-1-[(2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-benzyloxymethoxy-hexadecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxycarbonylmethyl]-dodecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 126024-96-2
(R)-3-Benzyloxymethoxy-tetradecanoic acid (R)-1-[(4aR,6R,7R,8R,8aS)-6-benzyloxy-7-((R)-3-benzyloxymethoxy-hexadecanoylamino)-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxycarbonylmethyl]-dodecyl ester

: 126024-97-3
(R)-3-Benzyloxymethoxy-tetradecanoic acid (R)-1-[(2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-benzyloxymethoxy-hexadecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxycarbonylmethyl]-dodecyl ester

Guidance literature:: With acetic acid; In water; at 45 ℃; for 1h;
DOI:10.1271/bbb.59.1790

Reference yield:

: (R)-3-Benzyloxymethoxy-hexadecanoic acid

: 126024-97-3
(R)-3-Benzyloxymethoxy-tetradecanoic acid (R)-1-[(2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-benzyloxymethoxy-hexadecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxycarbonylmethyl]-dodecyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / 1-(3-dimethylaminipropyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / Ambient temperature

2: 93 percent / DMAP, WSC / CH₂Cl₂ / 2 h / Ambient temperature

3: 80 percent / acetic acid / H₂O / 1 h / 45 °C

With dmap; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; water;
DOI:10.1271/bbb.59.1790

Reference yield:

: 126004-88-4
(R)-3-Benzyloxymethoxy-hexadecanoic acid ((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-amide

: 126024-97-3
(R)-3-Benzyloxymethoxy-tetradecanoic acid (R)-1-[(2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-benzyloxymethoxy-hexadecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxycarbonylmethyl]-dodecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / DMAP, WSC / CH₂Cl₂ / 2 h / Ambient temperature

2: 80 percent / acetic acid / H₂O / 1 h / 45 °C

With dmap; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; water;
DOI:10.1271/bbb.59.1790