(R)-3-Benzyloxymethoxy-hexadecanoic acid ((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-amide

Base Information

Chemical Name:(R)-3-Benzyloxymethoxy-hexadecanoic acid ((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-amide
CAS No.:126004-88-4
Molecular Formula:C₄₀H₆₁NO₈
Molecular Weight:683.926
Hs Code.:

Synonyms:(R)-3-Benzyloxymethoxy-hexadecanoic acid ((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-3-Benzyloxymethoxy-hexadecanoic acid ((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-amide

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Technology Process of (R)-3-Benzyloxymethoxy-hexadecanoic acid ((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-amide

There total 1 articles about (R)-3-Benzyloxymethoxy-hexadecanoic acid ((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 102794-17-2
benzyl 2-amino-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

: (R)-3-Benzyloxymethoxy-hexadecanoic acid

: 126004-88-4
(R)-3-Benzyloxymethoxy-hexadecanoic acid ((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-amide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; Ambient temperature;
DOI:10.1271/bbb.59.1790

Reference yield: 93.0%

: (3R)-3-<(3R)-3-(benzyloxymethoxy)tetradecanoyloxy>tetradecanoic acid

: 126004-88-4
(R)-3-Benzyloxymethoxy-hexadecanoic acid ((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-amide

: 126024-96-2
(R)-3-Benzyloxymethoxy-tetradecanoic acid (R)-1-[(4aR,6R,7R,8R,8aS)-6-benzyloxy-7-((R)-3-benzyloxymethoxy-hexadecanoylamino)-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxycarbonylmethyl]-dodecyl ester

Guidance literature:: With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1271/bbb.59.1790

Reference yield:

: 126004-88-4
(R)-3-Benzyloxymethoxy-hexadecanoic acid ((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-amide

: 126024-97-3
(R)-3-Benzyloxymethoxy-tetradecanoic acid (R)-1-[(2R,3R,4R,5S,6R)-2-benzyloxy-3-((R)-3-benzyloxymethoxy-hexadecanoylamino)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxycarbonylmethyl]-dodecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / DMAP, WSC / CH₂Cl₂ / 2 h / Ambient temperature

2: 80 percent / acetic acid / H₂O / 1 h / 45 °C

With dmap; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; water;
DOI:10.1271/bbb.59.1790