3,21-dichloro-11,13,29,31-tetramethyl-12,30-diphenyl-2,4,20,22-tetraoxa-10,11,13,14,28,29,31,32-octaaza-3,12,21,30-tetraphosphapentacyclo<32.2.2.2^5,8.2^16,19.2^23,25>tetratetraconta-5,7,9,14,16,18,23,25,27,32,34,36,37,39,41,43-hexadecene 3,12,21,...

Base Information

• Chemical Name: 3,21-dichloro-11,13,29,31-tetramethyl-12,30-diphenyl-2,4,20,22-tetraoxa-10,11,13,14,28,29,31,32-octaaza-3,12,21,30-tetraphosphapentacyclo<32.2.2.2^5,8.2^16,19.2^23,25>tetratetraconta-5,7,9,14,16,18,23,25,27,32,34,36,37,39,41,43-hexadecene 3,12,21,...
• CAS No.: 135799-41-6
• Molecular Formula: C₄₄H₄₂Cl₂N₈O₄P₄S₄
• Molecular Weight: 1069.93

Synonyms:3,21-dichloro-11,13,29,31-tetramethyl-12,30-diphenyl-2,4,20,22-tetraoxa-10,11,13,14,28,29,31,32-octaaza-3,12,21,30-tetraphosphapentacyclo<32.2.2.2^5,8.2^16,19.2^23,25>tetratetraconta-5,7,9,14,16,18,23,25,27,32,34,36,37,39,41,43-hexadecene 3,12,21,...

Chemical Property of 3,21-dichloro-11,13,29,31-tetramethyl-12,30-diphenyl-2,4,20,22-tetraoxa-10,11,13,14,28,29,31,32-octaaza-3,12,21,30-tetraphosphapentacyclo<32.2.2.2^5,8.2^16,19.2^23,25>tetratetraconta-5,7,9,14,16,18,23,25,27,32,34,36,37,39,41,43-hexadecene 3,12,21,...

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Technology Process of 3,21-dichloro-11,13,29,31-tetramethyl-12,30-diphenyl-2,4,20,22-tetraoxa-10,11,13,14,28,29,31,32-octaaza-3,12,21,30-tetraphosphapentacyclo<32.2.2.2^5,8.2^16,19.2^23,25>tetratetraconta-5,7,9,14,16,18,23,25,27,32,34,36,37,39,41,43-hexadecene 3,12,21,...

There total 2 articles about 3,21-dichloro-11,13,29,31-tetramethyl-12,30-diphenyl-2,4,20,22-tetraoxa-10,11,13,14,28,29,31,32-octaaza-3,12,21,30-tetraphosphapentacyclo<32.2.2.2^5,8.2^16,19.2^23,25>tetratetraconta-5,7,9,14,16,18,23,25,27,32,34,36,37,39,41,43-hexadecene 3,12,21,... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

phenylthiophosphodi(methylhydrazide) (54529-68-9) + bis(4-formylphenyl) chlorothiophosphonate (135799-32-5) → 3,21-dichloro-11,13,29,31-tetramethyl-12,30-diphenyl-2,4,20,22-tetraoxa-10,11,13,14,28,29,31,32-octaaza-3,12,21,30-tetraphosphapentacyclo<32.2.2.25,8.216,19.223,25>tetratetraconta-5,7,9,14,16,18,23,25,27,32,34,36,37,39,41,43-hexadecene 3,12,21,... (135799-41-6)

Guidance literature:

With 4 A molecular sieve; In tetrahydrofuran; -80 deg C to RT, 4 h;

DOI:10.1055/s-1995-4020

Reference yield: 60.0%

PS(C6H5)(N(CH3)NCHC6H4OH)2 (135831-40-2) → 3,21-dichloro-11,13,29,31-tetramethyl-12,30-diphenyl-2,4,20,22-tetraoxa-10,11,13,14,28,29,31,32-octaaza-3,12,21,30-tetraphosphapentacyclo<32.2.2.25,8.216,19.223,25>tetratetraconta-5,7,9,14,16,18,23,25,27,32,34,36,37,39,41,43-hexadecene 3,12,21,... (135799-41-6)

Guidance literature:

With triethylamine; trichlorophosphate; In tetrahydrofuran; -80 deg C to RT, 3 h;

DOI:10.1055/s-1995-4020

Reference yield: 95.0%

3,21-dichloro-11,13,29,31-tetramethyl-12,30-diphenyl-2,4,20,22-tetraoxa-10,11,13,14,28,29,31,32-octaaza-3,12,21,30-tetraphosphapentacyclo<32.2.2.25,8.216,19.223,25>tetratetraconta-5,7,9,14,16,18,23,25,27,32,34,36,37,39,41,43-hexadecene 3,12,21,... (135799-41-6) → 3,21-diazido-11,13,29,31-tetramethyl-12,30-diphenyl-2,4,20,22-tetraoxa-10,11,13,14,28,29,31,32-octaaza-3,12,21,30-tetraphosphapentacyclo<32.2.2.25,8.216,19.223,26>tetratetraconta-5,7,9,14,16,18,23,25,27,32,34,36,37,39,41,43-hexadecene 3,12,21,3... (156457-80-6)

Guidance literature:

With sodium azide; In tetrahydrofuran; Ambient temperature;

DOI:10.1055/s-1995-4020

upstream raw materials:

phenylthiophosphodi(methylhydrazide)

bis(4-formylphenyl) chlorothiophosphonate

PS(C₆H₅)(N(CH₃)NCHC₆H₄OH)2

Downstream raw materials:

3,21-diazido-11,13,29,31-tetramethyl-12,30-diphenyl-2,4,20,22-tetraoxa-10,11,13,14,28,29,31,32-octaaza-3,12,21,30-tetraphosphapentacyclo<32.2.2.2^5,8.2^16,19.2^23,26>tetratetraconta-5,7,9,14,16,18,23,25,27,32,34,36,37,39,41,43-hexadecene 3,12,21,3...

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