L-N-Z-5-(benzyloxy)tryptophyl-L-γ-methyl-N-<2-(5-methoxy-3-indolyl)ethyl>isoglutamide

Base Information

Chemical Name:L-N-Z-5-(benzyloxy)tryptophyl-L-γ-methyl-N-<2-(5-methoxy-3-indolyl)ethyl>isoglutamide
CAS No.:150184-24-0
Molecular Formula:C₄₃H₄₅N₅O₈
Molecular Weight:759.859
Hs Code.:

Synonyms:L-N-Z-5-(benzyloxy)tryptophyl-L-γ-methyl-N-<2-(5-methoxy-3-indolyl)ethyl>isoglutamide

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Chemical Property of L-N-Z-5-(benzyloxy)tryptophyl-L-γ-methyl-N-<2-(5-methoxy-3-indolyl)ethyl>isoglutamide

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Technology Process of L-N-Z-5-(benzyloxy)tryptophyl-L-γ-methyl-N-<2-(5-methoxy-3-indolyl)ethyl>isoglutamide

There total 6 articles about L-N-Z-5-(benzyloxy)tryptophyl-L-γ-methyl-N-<2-(5-methoxy-3-indolyl)ethyl>isoglutamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 3520-59-0
L-N-benzyloxycarbonyl-5-benzyloxytryptophan

: 150184-25-1
L-γ-methyl-N-<2-(5-methoxy-3-indolyl)ethyl>isoglutamide

: 150184-24-0
L-N-Z-5-(benzyloxy)tryptophyl-L-γ-methyl-N-<2-(5-methoxy-3-indolyl)ethyl>isoglutamide

Guidance literature:: With pyridine; dicyclohexyl-carbodiimide; In acetonitrile; at 0 - 16 ℃; for 97h;

Reference yield:

: 608-07-1
2-(5-methoxyindol-3-yl)ethylamine

: 150184-24-0
L-N-Z-5-(benzyloxy)tryptophyl-L-γ-methyl-N-<2-(5-methoxy-3-indolyl)ethyl>isoglutamide

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / dicyclohexylcarbodiimide / acetonitrile / 49 h / 0 - 5 °C

2: H₂ / Pd/C / methanol / 24 h / Heating

3: 67 percent / dicyclohexylcarbodiimide, pyridine / acetonitrile / 97 h / 0 - 16 °C

With pyridine; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; acetonitrile;

Reference yield:

: 4652-65-7
(S)-2-Benzyloxycarbonylamino-pentanedioic acid 5-methyl ester

: 150184-24-0
L-N-Z-5-(benzyloxy)tryptophyl-L-γ-methyl-N-<2-(5-methoxy-3-indolyl)ethyl>isoglutamide

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / dicyclohexylcarbodiimide / acetonitrile / 49 h / 0 - 5 °C

2: H₂ / Pd/C / methanol / 24 h / Heating

3: 67 percent / dicyclohexylcarbodiimide, pyridine / acetonitrile / 97 h / 0 - 16 °C

With pyridine; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; acetonitrile;