N-<<<(2,4-diaminopteridin-6-yl)methyl>amino>benzyl>-N-formyl-L-glutamic acid

Base Information

Chemical Name:N-<<<(2,4-diaminopteridin-6-yl)methyl>amino>benzyl>-N-formyl-L-glutamic acid
CAS No.:83314-88-9
Molecular Formula:C₂₀H₂₂N₈O₅
Molecular Weight:454.445
Hs Code.:

Synonyms:N-<<<(2,4-diaminopteridin-6-yl)methyl>amino>benzyl>-N-formyl-L-glutamic acid

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Chemical Property of N-<<<(2,4-diaminopteridin-6-yl)methyl>amino>benzyl>-N-formyl-L-glutamic acid

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Technology Process of N-<<<(2,4-diaminopteridin-6-yl)methyl>amino>benzyl>-N-formyl-L-glutamic acid

There total 4 articles about N-<<<(2,4-diaminopteridin-6-yl)methyl>amino>benzyl>-N-formyl-L-glutamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83334-49-0
diethyl N-formyl-N-(p-nitrobenzyl)-L-glutamate

: 83314-88-9
N-<<<(2,4-diaminopteridin-6-yl)methyl>amino>benzyl>-N-formyl-L-glutamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / H₂ / 5percent Pd/C / ethanol

2: 59 percent / K₂CO₃ / N,N-dimethyl-acetamide / 168 h / Ambient temperature

3: Ba(OH)2*8H₂O / ethanol; H₂O

With barium dihydroxide; hydrogen; potassium carbonate; palladium on activated charcoal; In ethanol; N,N-dimethyl acetamide; water;
DOI:10.1021/jm00354a013

Reference yield:

: 83314-84-5
diethyl N-(p-nitrobenzyl)-L-glutamate hydrochloride salt

: 83314-88-9
N-<<<(2,4-diaminopteridin-6-yl)methyl>amino>benzyl>-N-formyl-L-glutamic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / N,N'-dicyclohexylcarbodiimide, Et₃N, pyridine / CHCl₃

2: 78 percent / H₂ / 5percent Pd/C / ethanol

3: 59 percent / K₂CO₃ / N,N-dimethyl-acetamide / 168 h / Ambient temperature

4: Ba(OH)2*8H₂O / ethanol; H₂O

With pyridine; barium dihydroxide; hydrogen; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; chloroform; N,N-dimethyl acetamide; water;
DOI:10.1021/jm00354a013