C₅₁H₆₉N₅O₁₁

Base Information

Chemical Name:C₅₁H₆₉N₅O₁₁
CAS No.:484673-82-7
Molecular Formula:C₅₁H₆₉N₅O₁₁
Molecular Weight:928.136
Hs Code.:

C<sub>51</sub>H<sub>69</sub>N<sub>5</sub>O<sub>11</sub>

Synonyms:C₅₁H₆₉N₅O₁₁

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₁H₆₉N₅O₁₁

Chemical Property:

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Technology Process of C₅₁H₆₉N₅O₁₁

There total 17 articles about C₅₁H₆₉N₅O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 484671-61-6
Imidazole-1-carboxylic acid (E)-(2R,3S,7R,9R,10R,11R,13R)-10-((2S,3R,4S,6R)-3-benzoyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yloxy)-2-ethyl-9-methoxy-5,7,9,11,13-pentamethyl-6,12,14-trioxo-3-vinyl-oxacyclotetradec-4-en-3-yl ester

: 93-97-0
benzoic acid anhydride

: 173838-63-6
4-[4-(3-pyridyl)imidazol-1-yl]butylamine

: 484673-82-7
C₅₁H₆₉N₅O₁₁

Guidance literature:: Imidazole-1-carboxylic acid (E)-(2R,3S,7R,9R,10R,11R,13R)-10-((2S,3R,4S,6R)-3-benzoyloxy-4-dimethylamino-6-methyl-tetrahydro-pyran-2-yloxy)-2-ethyl-9-methoxy-5,7,9,11,13-pentamethyl-6,12,14-trioxo-3-vinyl-oxacyclotetradec-4-en-3-yl ester; 4-[4-(3-pyridyl)imidazol-1-yl]butylamine; In water; acetonitrile; at 65 ℃; for 14h;

benzoic acid anhydride; With dmap; triethylamine; In dichloromethane; for 12h;

Reference yield:

: 484670-62-4
C₅₅H₈₁NO₁₄

: 484673-82-7
C₅₁H₆₉N₅O₁₁

Guidance literature:: Multi-step reaction with 11 steps

1.1: 90 percent / pyridinium p-toluenesulfonate / acetonitrile; H₂O / 17 h / 68 °C

2.1: 82 percent / N-methylmorpholine N-oxide monohydrate; OsO₄ / acetone; 2-methyl-propan-2-ol; H₂O / 4 h / 20 °C

3.1: diisopropylethylamine; (dimethylamino)pyridine / CH₂Cl₂ / 17 h / -10 °C

4.1: 99 percent / Dess-Martin periodinane / CH₂Cl₂ / 14 h / 0 °C

5.1: 100 percent / pyridine / 18 h / 0 °C

6.1: 90 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / acetone / 45 h / 20 - 68 °C

7.1: 46.0 g / aq. HCl / 12 h / 40 °C

8.1: 99 percent / methyl sulfide; diisopropylethylamine; N-chlorosuccinimide / tetrahydrofuran / -15 - -10 °C

9.1: potassium bis(trimethylsilyl)amide / tetrahydrofuran; toluene / 1 h / -78 °C

9.2: 51 percent / tetrahydrofuran; toluene / 5 h / -78 - 20 °C

10.1: NaH / tetrahydrofuran / 7 h / 0 °C

11.1: acetonitrile; H₂O / 12 h / Heating

With pyridine; hydrogenchloride; dmap; N-chloro-succinimide; osmium(VIII) oxide; dimethylsulfide; pyridinium p-toluenesulfonate; potassium hexamethylsilazane; sodium hydride; Dess-Martin periodane; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; acetone; toluene; acetonitrile; tert-butyl alcohol; 4.1: Dess-Martin oxidation;
DOI:10.1021/jm051157a

Reference yield:

: 484671-59-2
Benzoic acid (2S,3R,4S,6R)-4-dimethylamino-2-((E)-(3R,5R,6R,7R,9R,13S,14R)-14-ethyl-13-formyl-13-hydroxy-7-methoxy-3,5,7,9,11-pentamethyl-2,4,10-trioxo-oxacyclotetradec-11-en-6-yloxy)-6-methyl-tetrahydro-pyran-3-yl ester

: 484673-82-7
C₅₁H₆₉N₅O₁₁

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium bis(trimethylsilyl)amide / tetrahydrofuran; toluene / 1 h / -78 °C

1.2: 51 percent / tetrahydrofuran; toluene / 5 h / -78 - 20 °C

2.1: NaH / tetrahydrofuran / 7 h / 0 °C

3.1: acetonitrile; H₂O / 12 h / Heating

With potassium hexamethylsilazane; sodium hydride; In tetrahydrofuran; water; toluene; acetonitrile;
DOI:10.1021/jm051157a