4-Biphenylyl disulfide

Base Information

Chemical Name:4-Biphenylyl disulfide
CAS No.:19813-92-4
Molecular Formula:C₂₄H₁₈S₂
Molecular Weight:370.539
Hs Code.:
DSSTox Substance ID:DTXSID00394416
Nikkaji Number:J926.784K
Wikidata:Q82193786

Synonyms:4-BIPHENYLYL DISULFIDE;19813-92-4;1,2-Di([1,1'-biphenyl]-4-yl)disulfane;1,2-di(biphenyl-4-yl)disulfane;(4-phenyl)phenyldisulphide;Bis(4-biphenylyl) persulfide;SCHEMBL905406;DTXSID00394416;SXSGFEDKJPABJD-UHFFFAOYSA-N;AKOS025296430;4,4'-Disulfanediyldi(1,1'-biphenyl)

Suppliers and Price of 4-Biphenylyl disulfide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1,2-Di([1,1'-biphenyl]-4-yl)disulfane 97%
5g
$ 1086.00

Alichem
4-Biphenylyldisulfide
5g
$ 1209.60

Total 0 raw suppliers

Chemical Property of 4-Biphenylyl disulfide

Chemical Property:

XLogP3:7.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:370.08499292
Heavy Atom Count:26
Complexity:343

Purity/Quality:: 1,2-Di([1,1'-biphenyl]-4-yl)disulfane 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=CC=C(C=C2)SSC3=CC=C(C=C3)C4=CC=CC=C4

Technology Process of 4-Biphenylyl disulfide

There total 15 articles about 4-Biphenylyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 92-66-0
4-bromo-1,1'-biphenyl

: 19813-92-4
1,2-di([1,1'-biphenyl]-4-yl)disulfane

Guidance literature:: 4-bromo-1,1'-biphenyl; With magnesium; In tetrahydrofuran; ethylene dibromide; at 60 - 65 ℃; for 1h; Inert atmosphere;

With sulfur; In tetrahydrofuran; ethylene dibromide; at 60 - 65 ℃;

With dihydrogen peroxide; In tetrahydrofuran; ethylene dibromide; at 20 ℃; for 2h;

Reference yield: 81.0%

: 603-35-0
triphenylphosphine

: biphenyl-4-sulfinic acid sodium salt

: 19813-92-4
1,2-di([1,1'-biphenyl]-4-yl)disulfane

Guidance literature:: In N,N-dimethyl-formamide; at 100 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.1c02656

Reference yield: 78.0%

: 1623-93-4
4-diphenylsulfonyl chloride

: 19813-92-4
1,2-di([1,1'-biphenyl]-4-yl)disulfane

Guidance literature:: With tetra-(n-butyl)ammonium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 20h; chemoselective reaction;
DOI:10.1002/adsc.201600633