Technology Process of C39H49NO8Si
There total 6 articles about C39H49NO8Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / N,N-dimethyl-formamide / 5.5 h / 100 °C
2: triethylamine / dichloromethane / 0 - 20 °C
3: sodium acetate / tert-butyl alcohol / 31 h / 60 °C
4: sodium acetate; hydroxylamine hydrochloride / tetrahydrofuran; isopropyl alcohol; water / 1.5 h / 0 - 20 °C
5: triethylamine / chloroform / 3.5 h / 0 °C
6: chloroform / 24 h / 60 °C
With
hydroxylamine hydrochloride; sodium acetate; potassium carbonate; triethylamine;
In
tetrahydrofuran; dichloromethane; chloroform; water; N,N-dimethyl-formamide; isopropyl alcohol; tert-butyl alcohol;
DOI:10.1016/j.polymer.2013.06.020
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium acetate / tert-butyl alcohol / 31 h / 60 °C
2: sodium acetate; hydroxylamine hydrochloride / tetrahydrofuran; isopropyl alcohol; water / 1.5 h / 0 - 20 °C
3: triethylamine / chloroform / 3.5 h / 0 °C
4: chloroform / 24 h / 60 °C
With
hydroxylamine hydrochloride; sodium acetate; triethylamine;
In
tetrahydrofuran; chloroform; water; isopropyl alcohol; tert-butyl alcohol;
DOI:10.1016/j.polymer.2013.06.020