Technology Process of C25H25Cl2N3O3S
There total 7 articles about C25H25Cl2N3O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(x)C7H8O3S*C24H23Cl2N3O; methanesulfonyl chloride;
With
triethylamine;
In
2-methyltetrahydrofuran;
at 5 - 10 ℃;
for 1.5h;
With
sodium hydrogencarbonate;
In
2-methyltetrahydrofuran;
at 20 ℃;
for 0.1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 8 h / 125 °C
2.1: triethylamine; methanesulfonyl chloride / 2-methyltetrahydrofuran / 2 h / 5 °C
2.2: 4 h / 84 °C
3.1: 2-methyltetrahydrofuran; methanol / 5 h / -10 - 20 °C
4.1: triethylamine / 2-methyltetrahydrofuran / 1.5 h / 5 - 10 °C
4.2: 0.1 h / 20 °C
With
methanesulfonyl chloride; triethylamine;
In
2-methyltetrahydrofuran; methanol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: methanesulfonic acid / dichloromethane / 0.17 h / 10 - 16 °C
1.2: 1.5 h / 10 - 15 °C
1.3: 1 h / 5 - 10 °C
2.1: 8 h / 125 °C
3.1: triethylamine; methanesulfonyl chloride / 2-methyltetrahydrofuran / 2 h / 5 °C
3.2: 4 h / 84 °C
4.1: 2-methyltetrahydrofuran; methanol / 5 h / -10 - 20 °C
5.1: triethylamine / 2-methyltetrahydrofuran / 1.5 h / 5 - 10 °C
5.2: 0.1 h / 20 °C
With
methanesulfonic acid; methanesulfonyl chloride; triethylamine;
In
2-methyltetrahydrofuran; methanol; dichloromethane;