C₁₄H₁₈N₄O₂

Base Information

Chemical Name:C₁₄H₁₈N₄O₂
CAS No.:1612873-98-9
Molecular Formula:C₁₄H₁₈N₄O₂
Molecular Weight:274.323
Hs Code.:

C<sub>14</sub>H<sub>18</sub>N<sub>4</sub>O<sub>2</sub>

Synonyms:C₁₄H₁₈N₄O₂

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Chemical Property of C₁₄H₁₈N₄O₂

Chemical Property:

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Technology Process of C₁₄H₁₈N₄O₂

There total 5 articles about C₁₄H₁₈N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1612873-97-8
C₁₀H₁₄N₄

: 922-67-8
propynoic acid methyl ester

: 1612873-98-9
C₁₄H₁₈N₄O₂

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; In ethanol; water; at 20 ℃; for 12h;
DOI:10.1002/ejoc.201301838

Reference yield:

: 1612873-96-7
2-iodo-6-nitro-4-tert-butylaniline

: 1612873-98-9
C₁₄H₁₈N₄O₂

Guidance literature:: Multi-step reaction with 4 steps

1: sodium nitrite; sulfuric acid / ethanol / 0 °C / Reflux

2: tin(II) chloride dihdyrate; ethanol / Reflux

3: sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(l) iodide; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 1 h / 20 °C

4: sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(ll) sulfate pentahydrate / ethanol; water / 12 h / 20 °C

With copper(l) iodide; sodium azide; copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tin(II) chloride dihdyrate; ethanol; sulfuric acid; N,N`-dimethylethylenediamine; sodium nitrite; In ethanol; water; dimethyl sulfoxide;
DOI:10.1002/ejoc.201301838

Reference yield:

: 1369827-82-6
C₁₀H₁₂INO₂

: 1612873-98-9
C₁₄H₁₈N₄O₂

Guidance literature:: Multi-step reaction with 3 steps

1: tin(II) chloride dihdyrate; ethanol / Reflux

2: sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(l) iodide; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 1 h / 20 °C

3: sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(ll) sulfate pentahydrate / ethanol; water / 12 h / 20 °C

With copper(l) iodide; sodium azide; copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tin(II) chloride dihdyrate; ethanol; N,N`-dimethylethylenediamine; In ethanol; water; dimethyl sulfoxide;
DOI:10.1002/ejoc.201301838