7,19-Bis-(toluene-4-sulfonyl)-1,7,13,19-tetraaza-bicyclo[11.11.5]nonacosane

Base Information

Chemical Name:7,19-Bis-(toluene-4-sulfonyl)-1,7,13,19-tetraaza-bicyclo[11.11.5]nonacosane
CAS No.:160320-54-7
Molecular Formula:C₃₉H₆₄N₄O₄S₂
Molecular Weight:717.094
Hs Code.:

Synonyms:7,19-Bis-(toluene-4-sulfonyl)-1,7,13,19-tetraaza-bicyclo[11.11.5]nonacosane

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Chemical Property of 7,19-Bis-(toluene-4-sulfonyl)-1,7,13,19-tetraaza-bicyclo[11.11.5]nonacosane

Chemical Property:

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Technology Process of 7,19-Bis-(toluene-4-sulfonyl)-1,7,13,19-tetraaza-bicyclo[11.11.5]nonacosane

There total 9 articles about 7,19-Bis-(toluene-4-sulfonyl)-1,7,13,19-tetraaza-bicyclo[11.11.5]nonacosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 160320-53-6
7,19-Bis-(toluene-4-sulfonyl)-1,7,13,19-tetraaza-bicyclo[11.11.5]nonacosane-25,29-dione

: 160320-54-7
7,19-Bis-(toluene-4-sulfonyl)-1,7,13,19-tetraaza-bicyclo[11.11.5]nonacosane

Guidance literature:: With diborane; In tetrahydrofuran; for 7h; Heating;
DOI:10.1016/S0040-4039(00)74415-7

Reference yield:

: 5454-83-1
5-bromovaleric acid methyl ester

: 160320-54-7
7,19-Bis-(toluene-4-sulfonyl)-1,7,13,19-tetraaza-bicyclo[11.11.5]nonacosane

Guidance literature:: Multi-step reaction with 7 steps

1: 70 percent / butyllithium / tetrahydrofuran / 24 h / Heating

2: 60 percent / sodium hydroxide / ethanol; H₂O / 18 h / Heating

3: 95 percent / oxalyl chloride / benzene

4: 65 percent / toluene / 12 h / Ambient temperature

5: 95 percent / diborane / tetrahydrofuran

6: 60 percent / triethylamine / toluene

7: 80 percent / diborane / tetrahydrofuran / 7 h / Heating

With sodium hydroxide; n-butyllithium; oxalyl dichloride; triethylamine; diborane; In tetrahydrofuran; ethanol; water; toluene; benzene;
DOI:10.1016/S0040-4039(00)74415-7

Reference yield:

: 125683-07-0
methyl 5-(N-tosylamino)pentanoate

: 160320-54-7
7,19-Bis-(toluene-4-sulfonyl)-1,7,13,19-tetraaza-bicyclo[11.11.5]nonacosane

Guidance literature:: Multi-step reaction with 7 steps

1: 70 percent / butyllithium / tetrahydrofuran / 24 h / Heating

2: 60 percent / sodium hydroxide / ethanol; H₂O / 18 h / Heating

3: 95 percent / oxalyl chloride / benzene

4: 65 percent / toluene / 12 h / Ambient temperature

5: 95 percent / diborane / tetrahydrofuran

6: 60 percent / triethylamine / toluene

7: 80 percent / diborane / tetrahydrofuran / 7 h / Heating

With sodium hydroxide; n-butyllithium; oxalyl dichloride; triethylamine; diborane; In tetrahydrofuran; ethanol; water; toluene; benzene;
DOI:10.1016/S0040-4039(00)74415-7