N⁴-{3-nitro-4-[2-(5-sulfanyl-1,3,4-thiadiazol-2-yl)-1-diazenyl]phenyl}-4-morpholinecarboxamide

Base Information

• Chemical Name: N⁴-{3-nitro-4-[2-(5-sulfanyl-1,3,4-thiadiazol-2-yl)-1-diazenyl]phenyl}-4-morpholinecarboxamide
• CAS No.: 1419786-62-1
• Molecular Formula: C₁₃H₁₃N₇O₄S₂
• Molecular Weight: 395.423

Synonyms:N⁴-{3-nitro-4-[2-(5-sulfanyl-1,3,4-thiadiazol-2-yl)-1-diazenyl]phenyl}-4-morpholinecarboxamide

Chemical Property of N⁴-{3-nitro-4-[2-(5-sulfanyl-1,3,4-thiadiazol-2-yl)-1-diazenyl]phenyl}-4-morpholinecarboxamide

Chemical Property:

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Technology Process of N⁴-{3-nitro-4-[2-(5-sulfanyl-1,3,4-thiadiazol-2-yl)-1-diazenyl]phenyl}-4-morpholinecarboxamide

There total 2 articles about N⁴-{3-nitro-4-[2-(5-sulfanyl-1,3,4-thiadiazol-2-yl)-1-diazenyl]phenyl}-4-morpholinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

C11H13N3O4 (200422-12-4) + 2-Amino-5-mercapto-1,3,4-thiadiazole (2349-67-9) → N4-{3-nitro-4-[2-(5-sulfanyl-1,3,4-thiadiazol-2-yl)-1-diazenyl]phenyl}-4-morpholinecarboxamide (1419786-62-1)

Guidance literature:

2-Amino-5-mercapto-1,3,4-thiadiazole; With hydrogenchloride; sodium carbonate; sodium nitrite; In water; at 0 ℃;

C₁₁H₁₃N₃O₄; In water; for 1h;

DOI:10.14233/ajchem.2013.13227

Reference yield:

4-morpholinocarbonyl chloride (15159-40-7) + 3-nitro-aniline (99-09-2) → N4-{3-nitro-4-[2-(5-sulfanyl-1,3,4-thiadiazol-2-yl)-1-diazenyl]phenyl}-4-morpholinecarboxamide (1419786-62-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 0.33 h / Reflux

2.1: sodium nitrite; hydrogenchloride; sodium carbonate / water / 0 °C

2.2: 1 h

With hydrogenchloride; sodium carbonate; sodium nitrite; In water;

DOI:10.14233/ajchem.2013.13227

upstream raw materials:

C₁₁H₁₃N₃O₄

2-Amino-5-mercapto-1,3,4-thiadiazole

4-morpholinocarbonyl chloride

3-nitro-aniline

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