Technology Process of C51H73ClN2O9Si2
There total 5 articles about C51H73ClN2O9Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
at 40 ℃;
for 24h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: diisobutylaluminium hydride / dichloromethane / 0.5 h / -78 °C
2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 0.75 h / 23 °C
3.1: lithium diisopropyl amide / tetrahydrofuran / 0.08 h / -78 °C
3.2: 0.25 h / -78 °C
4.1: pyridine / 24 h / 40 °C
With
pyridine; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.08 h / -78 °C
1.2: 0.25 h / -78 °C
2.1: pyridine / 24 h / 40 °C
With
pyridine; lithium diisopropyl amide;
In
tetrahydrofuran;
