(Z)-3-[2-(4-Methoxy-phenyl)-ethylsulfanyl]-but-2-enoic acid methyl ester

Base Information

Chemical Name:(Z)-3-[2-(4-Methoxy-phenyl)-ethylsulfanyl]-but-2-enoic acid methyl ester
CAS No.:132004-90-1
Molecular Formula:C₁₄H₁₈O₃S
Molecular Weight:266.361
Hs Code.:

Synonyms:(Z)-3-[2-(4-Methoxy-phenyl)-ethylsulfanyl]-but-2-enoic acid methyl ester

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Chemical Property of (Z)-3-[2-(4-Methoxy-phenyl)-ethylsulfanyl]-but-2-enoic acid methyl ester

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Technology Process of (Z)-3-[2-(4-Methoxy-phenyl)-ethylsulfanyl]-but-2-enoic acid methyl ester

There total 4 articles about (Z)-3-[2-(4-Methoxy-phenyl)-ethylsulfanyl]-but-2-enoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.2%

: 63659-59-6
2-(4-methoxyphenyl)ethyl mercaptan

: 105-45-3
acetoacetic acid methyl ester

: 132004-90-1
(Z)-3-[2-(4-Methoxy-phenyl)-ethylsulfanyl]-but-2-enoic acid methyl ester

Guidance literature:: With toluene-4-sulfonic acid; In benzene; Heating;
DOI:10.3987/COM-89-5228

Reference yield:

: 104-01-8
4-Methoxyphenylacetic acid

: 132004-90-1
(Z)-3-[2-(4-Methoxy-phenyl)-ethylsulfanyl]-but-2-enoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / BH₃ / tetrahydrofuran / Ambient temperature

2: 95.2 percent / PBr₃ / benzene / Heating

3: 1.) thiourea, 2.) 3 N NaOH / 1.) EtOH, reflux, 2.) reflux

4: 95.2 percent / p-toluenesulfonic acid / benzene / Heating

With sodium hydroxide; borane; phosphorus tribromide; toluene-4-sulfonic acid; thiourea; In tetrahydrofuran; benzene;
DOI:10.3987/COM-89-5228

Reference yield:

: 14425-64-0
4-methoxyphenethyl bromide

: 132004-90-1
(Z)-3-[2-(4-Methoxy-phenyl)-ethylsulfanyl]-but-2-enoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) thiourea, 2.) 3 N NaOH / 1.) EtOH, reflux, 2.) reflux

2: 95.2 percent / p-toluenesulfonic acid / benzene / Heating

With sodium hydroxide; toluene-4-sulfonic acid; thiourea; In benzene;
DOI:10.3987/COM-89-5228