3-methyl-1-(2,6,6-trimethylcyclohex-1-en-1-yl)pent-1-en-4-yn-3-ol

Base Information

• Chemical Name: 3-methyl-1-(2,6,6-trimethylcyclohex-1-en-1-yl)pent-1-en-4-yn-3-ol
• CAS No.: 17075-53-5
• Molecular Formula: C₁₅H₂₂O
• Molecular Weight: 218.339
• Mol file: 17075-53-5.mol

Synonyms:3-methyl-1-(2,6,6-trimethylcyclohex-1-ene-yl)pent-1-ene-4-yn-3-ol

Chemical Property of 3-methyl-1-(2,6,6-trimethylcyclohex-1-en-1-yl)pent-1-en-4-yn-3-ol

Chemical Property:

• Vapor Pressure: 3.56E-05mmHg at 25°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-methyl-1-(2,6,6-trimethylcyclohex-1-en-1-yl)pent-1-en-4-yn-3-ol

There total 2 articles about 3-methyl-1-(2,6,6-trimethylcyclohex-1-en-1-yl)pent-1-en-4-yn-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-2-one (79-77-6,14901-07-6) + acetylenemagnesium bromide (4301-14-8) → 3-methyl-1-(2,6,6-trimethylcyclohex-1-ene-yl)pent-1-ene-4-yn-3-ol (17075-53-5)

Guidance literature:

4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-2-one; acetylenemagnesium bromide;

In water;

DOI:10.1515/znb-2018-0011

Reference yield:

→ 3-methyl-1-(2,6,6-trimethylcyclohex-1-ene-yl)pent-1-ene-4-yn-3-ol (17075-53-5)

Guidance literature:

Li-acetylid, β-Jonon;

Reference yield: 99.0%

1-Adamantanecarboxylic acid (828-51-3) + 3-methyl-1-(2,6,6-trimethylcyclohex-1-ene-yl)pent-1-ene-4-yn-3-ol (17075-53-5) → 3-hydroxy-3-methyl-5-(2,6,6-trimethylcyclohex-1-en-1-yl)penta-1,4-dien-1-yl adamantanoate

Guidance literature:

With bis(2-methylpropenyl)(1,2-bis(diphenylphosphino)ethane)ruthenium; In ethyl acetate; at 20 ℃; for 3h; Temperature; Inert atmosphere;

upstream raw materials:

4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-2-one

acetylenemagnesium bromide

Downstream raw materials:

2-[(E)-3-(1-methoxy-1-methyl-ethoxy)-3-methyl-pent-1-en-4-ynyl]-1,3,3-trimethyl-cyclohexene

3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2, 4-dienal

1-(2,6,6-trimethyl-1-cyclohexenyl)-3-methyl-3-methoxy-1-penten-4-yn