(2S,3R,4S,6S)-2-(2-(benzyloxy)ethyl)-6-(hydroxymethyl)-3-methyltetrahydro-2H-pyran-4-ol

Base Information

Chemical Name:(2S,3R,4S,6S)-2-(2-(benzyloxy)ethyl)-6-(hydroxymethyl)-3-methyltetrahydro-2H-pyran-4-ol
CAS No.:1350818-12-0
Molecular Formula:C₁₆H₂₄O₄
Molecular Weight:280.364
Hs Code.:

Synonyms:(2S,3R,4S,6S)-2-(2-(benzyloxy)ethyl)-6-(hydroxymethyl)-3-methyltetrahydro-2H-pyran-4-ol

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Chemical Property of (2S,3R,4S,6S)-2-(2-(benzyloxy)ethyl)-6-(hydroxymethyl)-3-methyltetrahydro-2H-pyran-4-ol

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Technology Process of (2S,3R,4S,6S)-2-(2-(benzyloxy)ethyl)-6-(hydroxymethyl)-3-methyltetrahydro-2H-pyran-4-ol

There total 4 articles about (2S,3R,4S,6S)-2-(2-(benzyloxy)ethyl)-6-(hydroxymethyl)-3-methyltetrahydro-2H-pyran-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 955044-11-8
C₆H₁₂O₂

: 19790-60-4
3-Benzyloxypropanal

: 1350818-12-0
(2S,3R,4S,6S)-2-(2-(benzyloxy)ethyl)-6-(hydroxymethyl)-3-methyltetrahydro-2H-pyran-4-ol

Guidance literature:: C₆H₁₂O₂; 3-Benzyloxypropanal; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 4h;

With methanol; potassium carbonate; at 20 ℃; for 2h; optical yield given as %de; stereoselective reaction;
DOI:10.1016/j.tetlet.2011.09.134

Reference yield:

: C₁₆H₂₄O₄*C₂HF₃O₂

: 1350818-12-0
(2S,3R,4S,6S)-2-(2-(benzyloxy)ethyl)-6-(hydroxymethyl)-3-methyltetrahydro-2H-pyran-4-ol

Guidance literature:: With potassium carbonate; In methanol; at 25 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.11.097

Reference yield:

: 19790-60-4
3-Benzyloxypropanal

: 1350818-12-0
(2S,3R,4S,6S)-2-(2-(benzyloxy)ethyl)-6-(hydroxymethyl)-3-methyltetrahydro-2H-pyran-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 3 h / 25 °C / Inert atmosphere

2: potassium carbonate / methanol / 0.5 h / 25 °C / Inert atmosphere

With potassium carbonate; In methanol; dichloromethane;
DOI:10.1016/j.tetlet.2014.11.097