dithiocarbonic acid S-[2,2-diethoxy-1-(2-oxo-cyclohexylmethyl)-ethyl] ester O-ethyl ester

Base Information

• Chemical Name: dithiocarbonic acid S-[2,2-diethoxy-1-(2-oxo-cyclohexylmethyl)-ethyl] ester O-ethyl ester
• CAS No.: 863643-16-7
• Molecular Formula: C₁₆H₂₈O₄S₂
• Molecular Weight: 348.528

Synonyms:dithiocarbonic acid S-[2,2-diethoxy-1-(2-oxo-cyclohexylmethyl)-ethyl] ester O-ethyl ester

Chemical Property of dithiocarbonic acid S-[2,2-diethoxy-1-(2-oxo-cyclohexylmethyl)-ethyl] ester O-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dithiocarbonic acid S-[2,2-diethoxy-1-(2-oxo-cyclohexylmethyl)-ethyl] ester O-ethyl ester

There total 1 articles about dithiocarbonic acid S-[2,2-diethoxy-1-(2-oxo-cyclohexylmethyl)-ethyl] ester O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

acrylaldehyde diethyl acetal (3054-95-3) + ethyl [(2-oxocyclohexyl)sulfanyl]methanethioate (82721-86-6) → dithiocarbonic acid S-[2,2-diethoxy-1-(2-oxo-cyclohexylmethyl)-ethyl] ester O-ethyl ester (863643-16-7)

Guidance literature:

With dilauryl peroxide; In 1,2-dichloro-ethane; Heating;

DOI:10.1021/ol051196g

Reference yield: 70.0%

dithiocarbonic acid S-[2,2-diethoxy-1-(2-oxo-cyclohexylmethyl)-ethyl] ester O-ethyl ester (863643-16-7) → 2-(3,3-diethoxypropyl)cyclohexanone (32520-52-8)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 100 ℃; for 1h;

DOI:10.1021/ol051196g

Reference yield:

dithiocarbonic acid S-[2,2-diethoxy-1-(2-oxo-cyclohexylmethyl)-ethyl] ester O-ethyl ester (863643-16-7) → 6-(3,3-diethoxy-propyl)-1-nitromethyl-cyclohexene

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / Bu₃SnH; AIBN / toluene / 1 h / 100 °C

2: N,N-dimethylethylenediamine / 12 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; N,N`-dimethylethylenediamine; In toluene;

DOI:10.1021/ol051196g

upstream raw materials:

acrylaldehyde diethyl acetal

ethyl [(2-oxocyclohexyl)sulfanyl]methanethioate

Downstream raw materials:

2-(3,3-diethoxypropyl)cyclohexanone

4-[6-(3,3-diethoxy-propyl)-cyclohex-1-enyl]-4-nitro-butyric acid methyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 863643-16-7 dithiocarbonic acid S-[2,2-diethoxy-1-(2-oxo-cyclohexylmethyl)-ethyl] ester O-ethyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send