2-iodobenzyl 3,3-dimethyl-1-butynyl sulfone

Base Information

Chemical Name:2-iodobenzyl 3,3-dimethyl-1-butynyl sulfone
CAS No.:1334033-28-1
Molecular Formula:C₁₃H₁₅IO₂S
Molecular Weight:362.231
Hs Code.:

Synonyms:2-iodobenzyl 3,3-dimethyl-1-butynyl sulfone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-iodobenzyl 3,3-dimethyl-1-butynyl sulfone

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Technology Process of 2-iodobenzyl 3,3-dimethyl-1-butynyl sulfone

There total 2 articles about 2-iodobenzyl 3,3-dimethyl-1-butynyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1334032-81-3
2-iodobenzyl 3,3-dimethyl-1-butynyl sulfide

: 1334033-28-1
2-iodobenzyl 3,3-dimethyl-1-butynyl sulfone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 6 ℃; Inert atmosphere;
DOI:10.1021/ol202196y

Reference yield:

: 917-92-0
3,3-Dimethylbut-1-yne

: 152418-10-5
o-iodobenzyl thiocyanate

: 1334033-28-1
2-iodobenzyl 3,3-dimethyl-1-butynyl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 6 °C / Inert atmosphere

With n-butyllithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol202196y