o-iodobenzyl thiocyanate

Base Information

Chemical Name:o-iodobenzyl thiocyanate
CAS No.:152418-10-5
Molecular Formula:C₈H₆INS
Molecular Weight:275.113
Hs Code.:

Synonyms:o-iodobenzyl thiocyanate

Suppliers and Price of o-iodobenzyl thiocyanate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of o-iodobenzyl thiocyanate

Chemical Property:

Purity/Quality:

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Technology Process of o-iodobenzyl thiocyanate

There total 2 articles about o-iodobenzyl thiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 40400-13-3
2-Iodobenzyl bromide

: 333-20-0
potassium thioacyanate

: 152417-92-0
2-iodobenzyl isothiocyanate

: 152418-10-5
o-iodobenzyl thiocyanate

Guidance literature:: With sodium iodide; In N,N-dimethyl-formamide; at 95 - 100 ℃; for 7h;
DOI:10.1016/S0040-4020(01)85758-6

Reference yield:

: 5159-41-1
2-iodobenzyl alcohol

: 152418-10-5
o-iodobenzyl thiocyanate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / thionyl bromide / CHCl₃ / 3 h / Heating

2: 12 percent / sodium iodide / dimethylformamide / 7 h / 95 - 100 °C

With sulfurous dibromide; sodium iodide; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85758-6