((2S,6S)-1,7-dioxaspiro[5.5]undec-4-en-2-ylmethoxy)(tert-butyl)diphenylsilane

Base Information

Chemical Name:((2S,6S)-1,7-dioxaspiro[5.5]undec-4-en-2-ylmethoxy)(tert-butyl)diphenylsilane
CAS No.:1093662-98-6
Molecular Formula:C₂₆H₃₄O₃Si
Molecular Weight:422.64
Hs Code.:

Synonyms:((2S,6S)-1,7-dioxaspiro[5.5]undec-4-en-2-ylmethoxy)(tert-butyl)diphenylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((2S,6S)-1,7-dioxaspiro[5.5]undec-4-en-2-ylmethoxy)(tert-butyl)diphenylsilane

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Technology Process of ((2S,6S)-1,7-dioxaspiro[5.5]undec-4-en-2-ylmethoxy)(tert-butyl)diphenylsilane

There total 2 articles about ((2S,6S)-1,7-dioxaspiro[5.5]undec-4-en-2-ylmethoxy)(tert-butyl)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1093662-96-4
(7R,9S)-10-((tert-butyldiphenylsilyl)oxy)dec-5-yne-1,7,9-triol

: 1093662-98-6
((2S,6S)-1,7-dioxaspiro[5.5]undec-4-en-2-ylmethoxy)(tert-butyl)diphenylsilane

Guidance literature:: With 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; silver trifluoromethanesulfonate; In tetrahydrofuran; at 0 ℃; for 0.333333h; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol802491m

Reference yield: 31.0%

: 1093663-02-5
(7R,9S)-10-(tert-butyldiphenylsilyloxy)dec-5-yne-1,7,9-triol

: 1093662-98-6
((2S,6S)-1,7-dioxaspiro[5.5]undec-4-en-2-ylmethoxy)(tert-butyl)diphenylsilane

: 1093663-04-7
(2S,4R,5S)-2-((tert-butyldiphenylsilyloxy)methyl)-1,6-dioxaspiro[4.6]undecan-4-ol

: 1093663-06-9
(2S,4R,5R)-2-((tert-butyldiphenylsilyloxy)methyl)-1,6-dioxaspiro[4.6]undecan-4-ol

Guidance literature:: With 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; silver trifluoromethanesulfonate; In tetrahydrofuran; at 0 ℃; for 0.333333h; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol802491m

Reference yield: 95.0%

: 1093662-98-6
((2S,6S)-1,7-dioxaspiro[5.5]undec-4-en-2-ylmethoxy)(tert-butyl)diphenylsilane

: 1093663-00-3
((2S,6S)-1,7-dioxaspiro[5.5]undecan-2-ylmethoxy)(tert-butyl)diphenylsilane

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 5.5h; under 760.051 Torr;
DOI:10.1021/ol802491m