(2S,3R,5S)-tetrahydro-5-((R)-oxiran-2-yl)-2-(trityloxymethyl)furan-3-yloxy-tert-butyldimethylsilane

Base Information

Chemical Name:(2S,3R,5S)-tetrahydro-5-((R)-oxiran-2-yl)-2-(trityloxymethyl)furan-3-yloxy-tert-butyldimethylsilane
CAS No.:1174714-32-9
Molecular Formula:C₃₂H₄₀O₄Si
Molecular Weight:516.753
Hs Code.:

Synonyms:(2S,3R,5S)-tetrahydro-5-((R)-oxiran-2-yl)-2-(trityloxymethyl)furan-3-yloxy-tert-butyldimethylsilane

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Chemical Property of (2S,3R,5S)-tetrahydro-5-((R)-oxiran-2-yl)-2-(trityloxymethyl)furan-3-yloxy-tert-butyldimethylsilane

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Technology Process of (2S,3R,5S)-tetrahydro-5-((R)-oxiran-2-yl)-2-(trityloxymethyl)furan-3-yloxy-tert-butyldimethylsilane

There total 1 articles about (2S,3R,5S)-tetrahydro-5-((R)-oxiran-2-yl)-2-(trityloxymethyl)furan-3-yloxy-tert-butyldimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1174714-31-8
(2S,3R,5S)-2-((trityloxy)methyl)-tetrahydro-5-((R)-oxiran-2-yl)furan-3-ol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1174714-32-9
(2S,3R,5S)-tetrahydro-5-((R)-oxiran-2-yl)-2-(trityloxymethyl)furan-3-yloxy-tert-butyldimethylsilane

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/jo900767x

Reference yield: 84.0%

: 14918-21-9
5-hexynonitrile

: 1174714-32-9
(2S,3R,5S)-tetrahydro-5-((R)-oxiran-2-yl)-2-(trityloxymethyl)furan-3-yloxy-tert-butyldimethylsilane

: 1174714-42-1
C₃₈H₄₇NO₄Si

Guidance literature:: 5-hexynonitrile; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.666667h;

(2S,3R,5S)-tetrahydro-5-((R)-oxiran-2-yl)-2-(trityloxymethyl)furan-3-yloxy-tert-butyldimethylsilane; With boron trifluoride diethyl etherate; In tetrahydrofuran; at -78 ℃; for 0.666667h;
DOI:10.1021/jo900767x