(1E,4E)-5-(furan-2-yl)-3-hydroxy-1-phenylpent-4-en-1-one O-methyl oxime

Base Information

Chemical Name:(1E,4E)-5-(furan-2-yl)-3-hydroxy-1-phenylpent-4-en-1-one O-methyl oxime
CAS No.:1361387-44-1
Molecular Formula:C₁₆H₁₇NO₃
Molecular Weight:271.316
Hs Code.:

Synonyms:(1E,4E)-5-(furan-2-yl)-3-hydroxy-1-phenylpent-4-en-1-one O-methyl oxime

Suppliers and Price of (1E,4E)-5-(furan-2-yl)-3-hydroxy-1-phenylpent-4-en-1-one O-methyl oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1E,4E)-5-(furan-2-yl)-3-hydroxy-1-phenylpent-4-en-1-one O-methyl oxime

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Technology Process of (1E,4E)-5-(furan-2-yl)-3-hydroxy-1-phenylpent-4-en-1-one O-methyl oxime

There total 1 articles about (1E,4E)-5-(furan-2-yl)-3-hydroxy-1-phenylpent-4-en-1-one O-methyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 39511-08-5
(E)-3-(2-furanyl)-2-propenal

: 15754-20-8
(E)-acetophenone O-methyloxime

: 1361387-44-1
(1E,4E)-5-(furan-2-yl)-3-hydroxy-1-phenylpent-4-en-1-one O-methyl oxime

Guidance literature:: (E)-acetophenone O-methyloxime; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

(E)-3-(2-furanyl)-2-propenal; In tetrahydrofuran; Inert atmosphere;
DOI:10.1021/ja300552c

Reference yield: 84.0%

: 1361387-44-1
(1E,4E)-5-(furan-2-yl)-3-hydroxy-1-phenylpent-4-en-1-one O-methyl oxime

: C₁₆H₁₅NO₃

Guidance literature:: With dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; at 45 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ja300552c

Reference yield:

: 1361387-44-1
(1E,4E)-5-(furan-2-yl)-3-hydroxy-1-phenylpent-4-en-1-one O-methyl oxime

: 1361387-97-4
(1E,5Z)-4-diazo-1-(furan-2-yl)-5-(methoxyimino)-5-phenylpent-1-en-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / 4 h / 45 °C / Inert atmosphere

2: 4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 3 h / 0 °C

With 4-toluenesulfonyl azide; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In acetonitrile;
DOI:10.1021/ja300552c