2-<2-ethoxycarbonyl-3,5-bis-(β-methoxyethoxymethoxy)phenyl>-4(E)-4-methylhex-4-en-3-one

Base Information

Chemical Name:2-<2-ethoxycarbonyl-3,5-bis-(β-methoxyethoxymethoxy)phenyl>-4(E)-4-methylhex-4-en-3-one
CAS No.:74149-68-1
Molecular Formula:C₂₄H₃₆O₉
Molecular Weight:468.544
Hs Code.:

Synonyms:2-<2-ethoxycarbonyl-3,5-bis-(β-methoxyethoxymethoxy)phenyl>-4(E)-4-methylhex-4-en-3-one

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Chemical Property of 2-<2-ethoxycarbonyl-3,5-bis-(β-methoxyethoxymethoxy)phenyl>-4(E)-4-methylhex-4-en-3-one

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Technology Process of 2-<2-ethoxycarbonyl-3,5-bis-(β-methoxyethoxymethoxy)phenyl>-4(E)-4-methylhex-4-en-3-one

There total 7 articles about 2-<2-ethoxycarbonyl-3,5-bis-(β-methoxyethoxymethoxy)phenyl>-4(E)-4-methylhex-4-en-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 344879-67-0
2,4-Bis-(2-methoxy-ethoxymethoxy)-6-((E)-3-methyl-2-oxo-pent-3-enyl)-benzoic acid ethyl ester

: 74-88-4
methyl iodide

: 74149-68-1
2-<2-ethoxycarbonyl-3,5-bis-(β-methoxyethoxymethoxy)phenyl>-4(E)-4-methylhex-4-en-3-one

Guidance literature:: With tetra(n-butyl)ammonium hydroxide; water; In dichloromethane; at 45 ℃; for 2h;

Reference yield:

: 497-03-0
2-methylbut-2-enal

: 74149-68-1
2-<2-ethoxycarbonyl-3,5-bis-(β-methoxyethoxymethoxy)phenyl>-4(E)-4-methylhex-4-en-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: ZnI₂

2: 88 percent / lithium di-isopropylamide / 1,2-dimethoxy-ethane; hexane / 1.) -78 deg C, 30 min, 2.) few minutes

3: tetraethylammonium fluoride, water / tetrahydrofuran / 0.5 h / Ambient temperature

4: 85 percent / tetrabutylammonium hydroxide, water / CH₂Cl₂ / 2 h / 45 °C

With tetra(n-butyl)ammonium hydroxide; water; tetraethylammonium fluoride; zinc(II) iodide; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dimethoxyethane; hexane; dichloromethane;

Reference yield:

: 71027-65-1
ethyl 2,4-dihydroxy-6-bromomethylbenzoate

: 74149-68-1
2-<2-ethoxycarbonyl-3,5-bis-(β-methoxyethoxymethoxy)phenyl>-4(E)-4-methylhex-4-en-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / sodium hydride / tetrahydrofuran / 15 h / -15 °C

2: 88 percent / lithium di-isopropylamide / 1,2-dimethoxy-ethane; hexane / 1.) -78 deg C, 30 min, 2.) few minutes

3: tetraethylammonium fluoride, water / tetrahydrofuran / 0.5 h / Ambient temperature

4: 85 percent / tetrabutylammonium hydroxide, water / CH₂Cl₂ / 2 h / 45 °C

With tetra(n-butyl)ammonium hydroxide; water; sodium hydride; tetraethylammonium fluoride; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dimethoxyethane; hexane; dichloromethane;