Technology Process of C40H43N5O15S4
There total 9 articles about C40H43N5O15S4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
acetic anhydride; acetic acid;
at 120 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium carbonate / N,N-dimethyl-formamide; water / 1 h / Inert atmosphere
1.2: 6.5 h / 100 °C / Inert atmosphere
2.1: hydrogenchloride; trifluoroacetic acid; sodium nitrite / water / 0.53 h / -10 - -5 °C
2.2: 4 h / 20 °C
2.3: pH 9
3.1: acetic acid / 3 h / 100 °C / Reflux
4.1: fuming sulphuric acid / 1 h / 20 °C
5.1: sulfolane / 1 h / 80 - 120 °C
6.1: acetic anhydride; acetic acid / 120 °C
With
sulfolane; hydrogenchloride; fuming sulphuric acid; acetic anhydride; sodium carbonate; acetic acid; trifluoroacetic acid; sodium nitrite;
In
water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride; trifluoroacetic acid; sodium nitrite / water / 0.53 h / -10 - -5 °C
1.2: 4 h / 20 °C
1.3: pH 9
2.1: acetic acid / 3 h / 100 °C / Reflux
3.1: fuming sulphuric acid / 1 h / 20 °C
4.1: sulfolane / 1 h / 80 - 120 °C
5.1: acetic anhydride; acetic acid / 120 °C
With
sulfolane; hydrogenchloride; fuming sulphuric acid; acetic anhydride; acetic acid; trifluoroacetic acid; sodium nitrite;
In
water;