4-(2,4-difluorophenyl)-piperazine-1-carboxylic acid 4-nitrophenyl ester

Base Information

Chemical Name:4-(2,4-difluorophenyl)-piperazine-1-carboxylic acid 4-nitrophenyl ester
CAS No.:1159598-37-4
Molecular Formula:C₁₇H₁₅F₂N₃O₄
Molecular Weight:363.321
Hs Code.:

Synonyms:4-(2,4-difluorophenyl)-piperazine-1-carboxylic acid 4-nitrophenyl ester

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Chemical Property of 4-(2,4-difluorophenyl)-piperazine-1-carboxylic acid 4-nitrophenyl ester

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Technology Process of 4-(2,4-difluorophenyl)-piperazine-1-carboxylic acid 4-nitrophenyl ester

There total 1 articles about 4-(2,4-difluorophenyl)-piperazine-1-carboxylic acid 4-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 7693-46-1
4-Nitrophenyl chloroformate

: 115761-79-0
1-(2,4-difluoro-phenyl)piperazine

: 1159598-37-4
4-(2,4-difluorophenyl)-piperazine-1-carboxylic acid 4-nitrophenyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

Reference yield: 100.0%

: 1159598-37-4
4-(2,4-difluorophenyl)-piperazine-1-carboxylic acid 4-nitrophenyl ester

: 135065-76-8
tert-butyl (2S)-2-(hydroxymethyl)morpholine-4-carboxylate

: 1159598-94-3
(2S)-[4-(2,4-difluoro-phenyl)-piperazine-1-carbonyloxymethyl]-morpholine-4-carboxylic acid tert-butyl ester

Guidance literature:: tert-butyl (2S)-2-(hydroxymethyl)morpholine-4-carboxylate; With sodium hydride; In tetrahydrofuran; for 0.5h;

4-(2,4-difluorophenyl)-piperazine-1-carboxylic acid 4-nitrophenyl ester; In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield: 86.0%

: 1159598-37-4
4-(2,4-difluorophenyl)-piperazine-1-carboxylic acid 4-nitrophenyl ester

: 135065-71-3
(R)-2-hydroxymethylmorpholine-4-carboxylic acid tert-butyl ester

: 1159598-97-6
(2R)-[4-(2,4-difluoro-phenyl)-piperazine-1-carbonyloxymethyl]-morpholine-4-carboxylic acid tert-butyl ester

Guidance literature:: (R)-2-hydroxymethylmorpholine-4-carboxylic acid tert-butyl ester; With sodium hydride; In tetrahydrofuran; for 0.5h;

4-(2,4-difluorophenyl)-piperazine-1-carboxylic acid 4-nitrophenyl ester; In tetrahydrofuran; at 20 ℃; for 24h;