C₂₁H₂₈BrNO₇

Base Information

Chemical Name:C₂₁H₂₈BrNO₇
CAS No.:1246559-97-6
Molecular Formula:C₂₁H₂₈BrNO₇
Molecular Weight:486.36
Hs Code.:

C<sub>21</sub>H<sub>28</sub>BrNO<sub>7</sub>

Synonyms:C₂₁H₂₈BrNO₇

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Chemical Property of C₂₁H₂₈BrNO₇

Chemical Property:

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Technology Process of C₂₁H₂₈BrNO₇

There total 7 articles about C₂₁H₂₈BrNO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 1246559-96-5
C₁₁H₁₂Br₂O₃

: 1246559-97-6
C₂₁H₂₈BrNO₇

Guidance literature:: With triethylamine; In ethyl acetate; at 20 ℃; for 2h;

Reference yield:

: 18640-58-9
3-nitro-4-bromoacetophenone

: 1246559-97-6
C₂₁H₂₈BrNO₇

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride; tin(ll) chloride / water; methanol / 3.5 h / 20 °C

2: sodium nitrite; tetrafluoroboric acid / water / 1 h / 0 °C

3: sulfuric acid / water / 0.5 h / Inert atmosphere; Reflux

4: potassium carbonate; potassium iodide / acetone / 96 h / 75 °C

5: bromine / chloroform / 2 h / 20 °C

6: triethylamine / ethyl acetate / 2 h / 20 °C

With hydrogenchloride; tetrafluoroboric acid; sulfuric acid; bromine; potassium carbonate; triethylamine; potassium iodide; tin(ll) chloride; sodium nitrite; In methanol; chloroform; water; ethyl acetate; acetone;

Reference yield:

: 99-90-1
para-bromoacetophenone

: 1246559-97-6
C₂₁H₂₈BrNO₇

Guidance literature:: Multi-step reaction with 7 steps

1: nitric acid / 0.5 h / 5 - 10 °C

2: hydrogenchloride; tin(ll) chloride / water; methanol / 3.5 h / 20 °C

3: sodium nitrite; tetrafluoroboric acid / water / 1 h / 0 °C

4: sulfuric acid / water / 0.5 h / Inert atmosphere; Reflux

5: potassium carbonate; potassium iodide / acetone / 96 h / 75 °C

6: bromine / chloroform / 2 h / 20 °C

7: triethylamine / ethyl acetate / 2 h / 20 °C

With hydrogenchloride; tetrafluoroboric acid; sulfuric acid; bromine; nitric acid; potassium carbonate; triethylamine; potassium iodide; tin(ll) chloride; sodium nitrite; In methanol; chloroform; water; ethyl acetate; acetone;