2-[(2-amino-6-oxo-1,4,5,6-tetrahydro-9H-purin-9-yl)methoxy]ethyl azidoacetate

Base Information

Chemical Name:2-[(2-amino-6-oxo-1,4,5,6-tetrahydro-9H-purin-9-yl)methoxy]ethyl azidoacetate
CAS No.:84499-68-3
Molecular Formula:C₁₀H₁₂N₈O₄
Molecular Weight:308.256
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(2-amino-6-oxo-1,4,5,6-tetrahydro-9H-purin-9-yl)methoxy]ethyl azidoacetate

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 2-[(2-amino-6-oxo-1,4,5,6-tetrahydro-9H-purin-9-yl)methoxy]ethyl azidoacetate

There total 2 articles about 2-[(2-amino-6-oxo-1,4,5,6-tetrahydro-9H-purin-9-yl)methoxy]ethyl azidoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 59277-89-3
acycloguanosine

: 30426-58-5
2-azidoacetyl chloride

: 84499-68-3
9-<<2-(azidoacetoxy)ethoxy>methyl>guanine

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 0 ℃; for 1h;
DOI:10.1021/jm00358a029

Reference yield:

: 59277-89-3
acycloguanosine

: 30426-58-5
2-azidoacetyl chloride

: 84499-68-3
9-<<2-(azidoacetoxy)ethoxy>methyl>guanine

: 84499-61-6
9-<<2-(glycyloxy)ethoxy>methyl>guanine hydrochloride

Guidance literature:: With sodium hydrogencarbonate; triethylamine; In N-methyl-acetamide; diethyl ether; ethanol; dichloromethane;

Reference yield: 65.0%

: 84499-68-3
9-<<2-(azidoacetoxy)ethoxy>methyl>guanine

: 84499-61-6
9-<<2-(glycyloxy)ethoxy>methyl>guanine hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; water; for 1.5h; under 2068.6 Torr;
DOI:10.1021/jm00358a029