(S)-ethyl 2-{[(1S)-1-(4-bromophenyl)-2,2,2-trifluoroethyl]amino}-4-methylpentanoate

Base Information

Chemical Name:(S)-ethyl 2-{[(1S)-1-(4-bromophenyl)-2,2,2-trifluoroethyl]amino}-4-methylpentanoate
CAS No.:1141929-15-8
Molecular Formula:C₁₆H₂₁BrF₃NO₂
Molecular Weight:396.247
Hs Code.:

Synonyms:(S)-ethyl 2-{[(1S)-1-(4-bromophenyl)-2,2,2-trifluoroethyl]amino}-4-methylpentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-ethyl 2-{[(1S)-1-(4-bromophenyl)-2,2,2-trifluoroethyl]amino}-4-methylpentanoate

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Technology Process of (S)-ethyl 2-{[(1S)-1-(4-bromophenyl)-2,2,2-trifluoroethyl]amino}-4-methylpentanoate

There total 3 articles about (S)-ethyl 2-{[(1S)-1-(4-bromophenyl)-2,2,2-trifluoroethyl]amino}-4-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2743-60-4,75023-21-1
L-Leucine ethyl ester

: 1112233-60-9
(1R)-1-(4-bromophenyl)-2,2,2-trifluoroethyl trifluoromethanesulfonate

: 1141929-15-8
(S)-ethyl 2-{[(1S)-1-(4-bromophenyl)-2,2,2-trifluoroethyl]amino}-4-methylpentanoate

Guidance literature:: With potassium carbonate; In cyclohexane; at 75 ℃; for 12h; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.tet.2008.12.064

Reference yield:

: 2743-60-4,75023-21-1
L-Leucine ethyl ester

: 1112233-60-9
(1R)-1-(4-bromophenyl)-2,2,2-trifluoroethyl trifluoromethanesulfonate

: (S)-ethyl 2-{[(1R)-1-(4-bromophenyl)-2,2,2-trifluoroethyl]amino}-4-methylpentanoate

: 1141929-15-8
(S)-ethyl 2-{[(1S)-1-(4-bromophenyl)-2,2,2-trifluoroethyl]amino}-4-methylpentanoate

Guidance literature:: With potassium carbonate; In cyclohexane; at 75 ℃; for 18h; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.tet.2008.12.064