(2S,3R,4R,5R)-5-benzylamino-1,3,4-O-tribenzyl-6-vinyl-1,2,3,4-hexanetetraol

Base Information

Chemical Name:(2S,3R,4R,5R)-5-benzylamino-1,3,4-O-tribenzyl-6-vinyl-1,2,3,4-hexanetetraol
CAS No.:440104-33-6
Molecular Formula:C₃₆H₄₁NO₄
Molecular Weight:551.726
Hs Code.:

Synonyms:(2S,3R,4R,5R)-5-benzylamino-1,3,4-O-tribenzyl-6-vinyl-1,2,3,4-hexanetetraol

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Chemical Property of (2S,3R,4R,5R)-5-benzylamino-1,3,4-O-tribenzyl-6-vinyl-1,2,3,4-hexanetetraol

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Technology Process of (2S,3R,4R,5R)-5-benzylamino-1,3,4-O-tribenzyl-6-vinyl-1,2,3,4-hexanetetraol

There total 10 articles about (2S,3R,4R,5R)-5-benzylamino-1,3,4-O-tribenzyl-6-vinyl-1,2,3,4-hexanetetraol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2S,3R,4R)-5-N-benzylhydroxylamino-1,3,4-O-tribenzyl-6-vinyl-1,2,3,4-hexanetetraol

: 440104-35-8
(2S,3R,4R,5S)-5-benzylamino-1,3,4-O-tribenzyl-6-vinyl-1,2,3,4-hexanetetraol

: 440104-33-6
(2S,3R,4R,5R)-5-benzylamino-1,3,4-O-tribenzyl-6-vinyl-1,2,3,4-hexanetetraol

Guidance literature:: With copper diacetate; acetic acid; zinc; In water; at 20 - 70 ℃; for 1h; Title compound not separated from byproducts;
DOI:10.1016/S0040-4020(03)00631-8

Reference yield:

: 2622-05-1
allylmagnesium bromide

: 192211-53-3
N-benzyl-2,3,5-tri-O-benzyl-L-xylofuranosylamine

: 440104-35-8
(2S,3R,4R,5S)-5-benzylamino-1,3,4-O-tribenzyl-6-vinyl-1,2,3,4-hexanetetraol

: 440104-33-6
(2S,3R,4R,5R)-5-benzylamino-1,3,4-O-tribenzyl-6-vinyl-1,2,3,4-hexanetetraol

Guidance literature:: In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0957-4166(02)00081-2

Reference yield:

: 100-39-0
benzyl bromide

: 440104-33-6
(2S,3R,4R,5R)-5-benzylamino-1,3,4-O-tribenzyl-6-vinyl-1,2,3,4-hexanetetraol

Guidance literature:: Multi-step reaction with 4 steps

1: 40 percent / Ba(OH)2 / dimethylformamide

2: 50 percent / aq. HCl / dioxane / Heating

3: 98 percent / 4 Angstroem molecular sieves / CH₂Cl₂

4: tetrahydrofuran / 0 °C

With hydrogenchloride; barium dihydroxide; 4 A molecular sieve; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0957-4166(02)00081-2