1-(2-(4-bromophenyl)-2-oxoethyl)-3-carbamoylpyridin-1-ium bromide

Base Information

• Chemical Name: 1-(2-(4-bromophenyl)-2-oxoethyl)-3-carbamoylpyridin-1-ium bromide
• CAS No.: 108749-69-5
• Molecular Formula: Br*C₁₄H₁₂BrN₂O₂
• Molecular Weight: 400.069
• Mol file: 108749-69-5.mol

Synonyms:1-(2-(4-bromophenyl)-2-oxoethyl)-3-carbamoylpyridin-1-ium bromide

Chemical Property of 1-(2-(4-bromophenyl)-2-oxoethyl)-3-carbamoylpyridin-1-ium bromide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-(2-(4-bromophenyl)-2-oxoethyl)-3-carbamoylpyridin-1-ium bromide

There total 1 articles about 1-(2-(4-bromophenyl)-2-oxoethyl)-3-carbamoylpyridin-1-ium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

nicotinamide (98-92-0,1255150-40-3) + para-bromophenacyl bromide (99-73-0,132309-76-3) → 1-(2-(4-bromophenyl)-2-oxoethyl)-3-carbamoylpyridin-1-ium bromide (108749-69-5)

Guidance literature:

In ethanol; for 0.166667h; Wavelength; Solvent; Temperature; Microwave irradiation;

DOI:10.3390/molecules24061001

Reference yield: 46.0%

1-(2-(4-bromophenyl)-2-oxoethyl)-3-carbamoylpyridin-1-ium bromide (108749-69-5) + 4-methoxy-aniline (104-94-9) → 3-(4-methoxyphenylcarbamoyl)-1-[2-oxo-2-(4-bromophenyl)ethyl]pyridinium bromide

Guidance literature:

1-(2-(4-bromophenyl)-2-oxoethyl)-3-carbamoylpyridin-1-ium bromide; 4-methoxy-aniline; With acetic acid; at 150 ℃; for 3h;

With hydrogen bromide;

DOI:10.1023/B:COHC.0000023782.49549.b6

Reference yield: 36.0%

1-(2-(4-bromophenyl)-2-oxoethyl)-3-carbamoylpyridin-1-ium bromide (108749-69-5) + E-1,2-dichloro-1,2-di(propylsulfonyl)ethene (118524-81-5) → 3-(4-bromobenzoyl)-1,2-bis(propylsulfonyl)indolizine-8-carboxamide

Guidance literature:

With triethylamine; In chloroform; at 50 ℃; for 0.666667h; regioselective reaction;

DOI:10.1007/s11172-017-1851-3

upstream raw materials:

nicotinamide

para-bromophenacyl bromide