P,P-dideuteriophenylphosphine pentacarbonyltungsten⁽⁰⁾

Base Information

Chemical Name:P,P-dideuteriophenylphosphine pentacarbonyltungsten⁽⁰⁾
CAS No.:875756-94-8
Molecular Formula:C₁₁H₇O₅PW
Molecular Weight:435.981
Hs Code.:

P,P-dideuteriophenylphosphine pentacarbonyltungsten<sup>(0)</sup>

Synonyms:P,P-dideuteriophenylphosphine pentacarbonyltungsten⁽⁰⁾

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Chemical Property of P,P-dideuteriophenylphosphine pentacarbonyltungsten⁽⁰⁾

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Technology Process of P,P-dideuteriophenylphosphine pentacarbonyltungsten⁽⁰⁾

There total 1 articles about P,P-dideuteriophenylphosphine pentacarbonyltungsten⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 61300-75-2
phenylphosphine pentacarbonyltungsten⁽⁰⁾

: 7789-20-0
water-d2

: 875756-94-8
P,P-dideuteriophenylphosphine pentacarbonyltungsten⁽⁰⁾

Guidance literature:: In tetrahydrofuran; (N2); D2O added to a soln. of W complex, stirred; evapd., pentane added, the D2O layer sepd., pentane evapd., the procedure repeated twice, the pentane layer filtered (Na2SO4), concd., crystd. at -20°C;
DOI:10.1021/ja054885w

Reference yield: 14.0%

: 875756-94-8
P,P-dideuteriophenylphosphine pentacarbonyltungsten⁽⁰⁾

: 21792-52-9
1,2-diethynylbenzene

: 872600-03-8
3-phenyl-1,5-dideuterio-3H-benzophosphenine pentacarbonyltungsten⁽⁰⁾

Guidance literature:: In tetrahydrofuran; (N2); 1,2-diethynylbenzene in THF added to a soln. of W complex, stirredfor 1 d at room temp. and 7 h at 35°C; filtered (silica), chromd. (toluene/pentane), crystd. at -20°C from Et2O/pentane;
DOI:10.1021/ja054885w