2-phenylhexanedinitrile

Base Information

Chemical Name:2-phenylhexanedinitrile
CAS No.:2941-39-1
Molecular Formula:C₁₂H₁₂N₂
Molecular Weight:184.241
Hs Code.:

Synonyms:2-phenylhexanedinitrile

Suppliers and Price of 2-phenylhexanedinitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-phenylhexanedinitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-phenylhexanedinitrile

There total 6 articles about 2-phenylhexanedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7677-24-9
trimethylsilyl cyanide

: 2-phenylcyclopentan-1-one O-(4-(trifluoromethyl)benzoyl)oxime

: 2941-39-1
2-phenylhexanedinitrile

Guidance literature:: With tetrakis(acetonitrile)copper(I) hexafluorophosphate; 10-phenyl-10H-phenothiazine; 4,4'-di-tert-butyl-2,2'-bipyridine; In N,N-dimethyl acetamide; at 30 ℃; Schlenk technique; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.9b03970

Reference yield:

: 83849-01-8
2-phenylcyclopentan-1-one oxime

: 2941-39-1
2-phenylhexanedinitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 °C / Inert atmosphere

2: 4,4'-di-tert-butyl-2,2'-bipyridine; 10-phenyl-10H-phenothiazine; tetrakis(acetonitrile)copper(I) hexafluorophosphate / N,N-dimethyl acetamide / 30 °C / Schlenk technique; Inert atmosphere; Irradiation

With dmap; tetrakis(acetonitrile)copper(I) hexafluorophosphate; 10-phenyl-10H-phenothiazine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4,4'-di-tert-butyl-2,2'-bipyridine; In dichloromethane; N,N-dimethyl acetamide;
DOI:10.1021/acs.orglett.9b03970

Reference yield:

: 120-92-3
cyclopentanone

: 2941-39-1
2-phenylhexanedinitrile

Guidance literature:: Multi-step reaction with 4 steps

1: palladium diacetate; tris-(o-tolyl)phosphine; sodium acetate; pyrrolidine; tert-Octylamine / 1,4-dioxane / 110 °C / Schlenk technique; Sealed tube

2: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 °C / Inert atmosphere

4: 4,4'-di-tert-butyl-2,2'-bipyridine; 10-phenyl-10H-phenothiazine; tetrakis(acetonitrile)copper(I) hexafluorophosphate / N,N-dimethyl acetamide / 30 °C / Schlenk technique; Inert atmosphere; Irradiation

With pyrrolidine; dmap; tetrakis(acetonitrile)copper(I) hexafluorophosphate; 10-phenyl-10H-phenothiazine; tert-Octylamine; hydroxylamine hydrochloride; sodium acetate; palladium diacetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tris-(o-tolyl)phosphine; 4,4'-di-tert-butyl-2,2'-bipyridine; sodium hydroxide; In 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl acetamide; water;
DOI:10.1021/acs.orglett.9b03970