[2,2'-[2,2-dimethyl-1,3-propanediylbis(nitrilomethylidyne)]bis(6-methoxyphenolato)^(2-)]nickel(II)

Base Information

• Chemical Name: [2,2'-[2,2-dimethyl-1,3-propanediylbis(nitrilomethylidyne)]bis(6-methoxyphenolato)^(2-)]nickel(II)
• CAS No.: 194716-60-4
• Molecular Formula: C₂₁H₂₄N₂O₄*Ni
• Molecular Weight: 427.123

Synonyms:[2,2'-[2,2-dimethyl-1,3-propanediylbis(nitrilomethylidyne)]bis(6-methoxyphenolato)^(2-)]nickel(II)

Chemical Property of [2,2'-[2,2-dimethyl-1,3-propanediylbis(nitrilomethylidyne)]bis(6-methoxyphenolato)^(2-)]nickel(II)

Chemical Property:

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Technology Process of [2,2'-[2,2-dimethyl-1,3-propanediylbis(nitrilomethylidyne)]bis(6-methoxyphenolato)^(2-)]nickel(II)

There total 1 articles about [2,2'-[2,2-dimethyl-1,3-propanediylbis(nitrilomethylidyne)]bis(6-methoxyphenolato)^(2-)]nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

nickel(II) nitrate hexahydrate + 2,2-Dimethyl-1,3-diaminopropane (7328-91-8) + 3-methoxy-2-hydroxybenzaldehyde (148-53-8) → [2,2'-[2,2-dimethyl-1,3-propanediylbis(nitrilomethylidyne)]bis(6-methoxyphenolato)(2-)]nickel(II) (194716-60-4)

Guidance literature:

With triethylamine; In ethanol; Reflux;

DOI:10.1016/j.ica.2017.06.058

Reference yield: 70.0%

potassium hexacyanochromate(III) (13601-11-1) + dysprosium(III) nitrate hexahydrate + [(N,N'-bis(3-methoxysalicylidene)-2,2-dimethyl-1,3-propanediamino)Ni(II)] (194716-60-4) + water (7732-18-5) + acetonitrile (75-05-8,26809-02-9) + 4-(3-phenylpropyl)pyridine-N-oxide (84824-92-0) → {[(N,N'-bis(3-methoxysalicylidene)-2,2-dimethyl-1,3-propanediamino)Ni(II)]2Dy(III)(H2O)Cr(III)(CN)6}2*24H2O*2CH3CN*2(4-(3-phenylpropyl)pyridine 1-oxide)

Guidance literature:

DOI:10.1039/c7dt00948h

upstream raw materials:

2,2-Dimethyl-1,3-diaminopropane

3-methoxy-2-hydroxybenzaldehyde

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