(E)-2-(4-hydroxy-3-methylbut-3-en-1-yl)-4-methoxy-1-methoxymethoxybenzene

Base Information

Chemical Name:(E)-2-(4-hydroxy-3-methylbut-3-en-1-yl)-4-methoxy-1-methoxymethoxybenzene
CAS No.:434928-87-7
Molecular Formula:C₁₄H₂₀O₄
Molecular Weight:252.31
Hs Code.:

Synonyms:(E)-2-(4-hydroxy-3-methylbut-3-en-1-yl)-4-methoxy-1-methoxymethoxybenzene

Suppliers and Price of (E)-2-(4-hydroxy-3-methylbut-3-en-1-yl)-4-methoxy-1-methoxymethoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(4-hydroxy-3-methylbut-3-en-1-yl)-4-methoxy-1-methoxymethoxybenzene

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Technology Process of (E)-2-(4-hydroxy-3-methylbut-3-en-1-yl)-4-methoxy-1-methoxymethoxybenzene

There total 8 articles about (E)-2-(4-hydroxy-3-methylbut-3-en-1-yl)-4-methoxy-1-methoxymethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 434928-86-6
(E)-2-(4-acetyloxy-3-methylbut-3-en-1-yl)-4-methoxy-1-methoxymethoxybenzene

: 434928-87-7
(E)-2-(4-hydroxy-3-methylbut-3-en-1-yl)-4-methoxy-1-methoxymethoxybenzene

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 2h;
DOI:10.1039/b110578g

Reference yield: 80.0%

: 307492-77-9
4-methoxy-1-(methoxymethoxy)-2-(3-methylbut-2-en-1-yl)benzene

: 434928-87-7
(E)-2-(4-hydroxy-3-methylbut-3-en-1-yl)-4-methoxy-1-methoxymethoxybenzene

Guidance literature:: 4-methoxy-1-(methoxymethoxy)-2-(3-methylbut-2-en-1-yl)benzene; With selenium(IV) oxide; In ethanol; for 0.5h; Heating;

With sodium tetrahydroborate; In ethanol; at 0 ℃; for 1h;
DOI:10.1002/1099-0690(200009)2000:18<3223::AID-EJOC3223>3.0.CO;2-L

Reference yield:

: 150-76-5
4-methoxy-phenol

: 434928-87-7
(E)-2-(4-hydroxy-3-methylbut-3-en-1-yl)-4-methoxy-1-methoxymethoxybenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / PdP(Ph₃)4 / CH₂Cl₂ / 4 h / 20 °C

2: 98 percent / dimethylaminopyridine; Et₃N / ethyl acetate / 4 h / 20 °C

3: 98 percent / HCl / CH₂Cl₂ / 0.03 h / 20 °C

4: 97 percent / (i-Pr)2NEt / CH₂Cl₂ / 12 h / 40 °C

5: 97 percent / aq. K₂CO₃ / methanol / 2 h / 20 °C

With hydrogenchloride; dmap; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; dichloromethane; ethyl acetate; 3: Claisen transposition;
DOI:10.1039/b110578g